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1.
醛与2,2—二羟甲基—1,3—丙二醇缩合制备了2,2—二羟甲基—1,3—丙二醇的二缩醛,并通过HNMR,IR和元素分析表征。  相似文献   

2.
2,2——二羟甲基—1,3——丙二醇与醛缩合制备了2,2——二羟甲基—1,3——丙二醇单缩醛,其产物通过~1HNMR,IR和元素分析表征。  相似文献   

3.
以十二醛与二羟甲基丙二酸二乙酯为原料反应,然后用氢氧化钠皂化,合成了2—正十—烷基—1,3—二氧杂环己烷—5,5—二羧酸二钠盐(4),并对它的临界胶束浓度(CMC)进行了测定。  相似文献   

4.
以1——十四醇和丙二酸二乙酯为原料,经三步反应首次合成了2——正十四烷基一1,3—丙二醇。  相似文献   

5.
研究了邻二—(二氯甲基)苯在冰乙酸条件下,滴加少量浓硫酸,酸解合成邻苯二甲醛各反应条件的影响;实验结果表明:邻二—(二氯甲基)苯与浓硫酸摩尔比为1:4,反应温度在90—100℃,反应时间为90min,邻苯二甲醛的收率可达92.3%.  相似文献   

6.
通过对—二甲基—2—苯基—1,4—氧氮杂—5,7—二酮的研究,表明这一化合物及其衍生物是手性源化合物,利用它合成许多手性化合物同时找到了合成1,4—氧氮杂的方法,产率较高.  相似文献   

7.
本文采用荧光熄灭法在水相中研究了席夫碱试剂l—(4—羟基水杨醛缩氨基)—8—羟基—3,6—萘二磺酸钠(HSHND)测定痕量Al(Ⅲ)的方法和条件。在PH=4.2的邻苯二甲酸氢钾缓冲体系中,试剂的激发波长λ_(ex)=356nm,荧炮发射波长λ_(em)=418nm,铝(Ⅲ)浓度在0.5—3.0μg/10mL范围内呈良好的线性关系,检出限为0.2μg/10mL。本法的灵敏度及选择性好,操作简便快速,无需加热。用于水样中痕量铝的测定,结果满意。  相似文献   

8.
研究了2—(3,5—二氯—2—吡啶偶氮)—5—二甲氨基苯胺与铑(Ⅲ)的显色反应,在PH4.0~5.2范围内,试剂与铑(Ⅲ)形成稳定的紫红色配合物、配合物形成后,提高酸度至0.72~mol.L~(-1)盐酸溶液,其中最大吸收峰红移至614nm,,灵敏度显著提高,表观摩尔吸光系数ε_(614)=1.40×10~5L·mol~(-1)、cm~(-1),铑含量在0~0.72μg、mol~(-1)内符合比尔定律。所拟方法操作简便,灵敏度高,用于储化剂中微量铑的测定,获得满意结果。  相似文献   

9.
合成了一种新的水溶性显色剂27(2—噻唑偶氮)—5—L(N.N—二羧甲基)氨基]苯磺酸(TADCABS)。利用红外光谱法和元素分析法测定了试剂的结构及组成。同时测定了试剂与28种金属离子的显色反应,其中6种离子能显色。  相似文献   

10.
本文研究了1.5—环辛二烯在AlCl_3或AlCl_3与和C_2H_5B_1催化下的聚合反应,并探讨了该反应的机理。  相似文献   

11.
Artificial intelligence (AI) refers to a type of algorithms or computerized systems that resemble human mental processes of decision making. Drawing upon multidisciplinary literature that intersects AI, decision making, educational leadership, and policymaking, this position paper aims to examine promising applications and potential perils of AI in educational leaders’ data-informed decision making (DIDM). Endowed with ever-growing computational power and real-time data, highly scalable AI can increase efficiency and accuracy in leaders’ DIDM. However, misusing AI can have perilous effects on education stakeholders. Many lurking biases in current AI could be amplified. Of more concern, the moral values (e.g., fairness, equity, honesty, and doing no harm) we uphold might clash with using AI to make data-informed decisions. Further, missteps on the issues about data security and privacy could have a life-long impact on stakeholders. The article concludes with recommendations for educational leaders to leverage AI potential and minimize its negative consequences.  相似文献   

12.
The concept of data-informed decision making (DIDM), a term used interchangeably with data-driven decision making (DDDM) and data-based decision making (DBDM), is relatively new to Irish education and the school planning process. This research sought to clarify what data principals use and how they use that information for school improvement considering new school self-evaluation requirements. The paper begins by charting the rise internationally of data use in school planning, decision making and accountability. It proceeds to describe the policy context in this area in Ireland and then reports recent research with school leaders around how data is collected and used in their work. Although the paper focusses on Ireland, it is tentatively suggested that school leaders, teachers and policymakers in other countries, and there are many, which have come late to the expectation that school improvement and accountability should be heavily data-informed may find the efforts of Irish principals in this regard of interest.  相似文献   

13.
焦化废水COD的无汞快速测定   总被引:1,自引:0,他引:1  
以硝酸银为Cl^-掩蔽剂,以硫酸银为催化剂,在11mol/L的硫酸及0.05mmol/L(1/6K2Cr2O7)K2Cr2O7介质中,COD测定的回流时间可统短至10min,样品的分析周期约为30min。此方法避免了使用剧毒硫酸汞产生的二次污染,回收、再用了废液中的银,进一步降低了分析费用,用于焦化废水COD的测定,结果与标准方法基本吻合。  相似文献   

14.
运用多媒体辅助教学中应处理好的几个关系   总被引:1,自引:0,他引:1  
随着多媒体辅助教学手段在高校教学中的广泛应用,教学手段、方法、观念、形式和评堂教学结构以及教学思想与教学理论都发生了改革,但是,如果没有处理好多媒体辅助教学与相关因素的关系,就难以达到预期理想的教学效果,为了能充分发挥多媒体辅助教学的优势作用应处理好多媒体硬件与软件的关系;处理好现代教学手段与传统教学手段的关系;处理好教师与多媒体设备的关系;处理好教学任务与课件信息内容的关系;处理好多媒体与其他教学媒体的关系:处理好教师与学生的关系;处理好课件的设计与课刊:制作的关系等。  相似文献   

15.
主要介绍了Grebner-Shirshov基理论的历史;回顾了自由李代数的合成钻石引进;找到了Lie(X;Ω)的一组线性基底;作为应用,证明了Lie(X;Ω)是带有多元算子的自由李代数.  相似文献   

16.
为提高细长轴车削加工质量,采用细长轴双刀车削加工方法,建立细长轴双刀车削加工模型,并对细长轴双刀车削进行理论分析.运用ANSYS软件对细长轴双刀车削加工和单刀车削加工进行静力学分析,通过比对二者仿真数据,得出细长轴双刀车削可以大幅度提高工件加工精度的结果,并验证双刀车削加工细长轴的可行性.  相似文献   

17.
通过比较KOH-Test法和革兰氏染色法,指出KOH-Test法是快速判定菌株的革兰氏染色反应的方法。  相似文献   

18.
本文通过介绍电主轴与直线电机结构和性能的优势,展示了在电主轴及直线电机装备下,当今国内外高速数控机床的新面貌,进而指出了我国高精、高速加工与国际间的差距,对我国高速数控机床产业提出几点建议,仅供同仁参考。  相似文献   

19.
This study explores the content validity of a profile used to describe the communication behaviour of people with intellectual disabilities. The profile, named Biala-II - a Wiradjuri (an Australian Aboriginal language) word for "I understand you" - makes use of the knowledge of informants who are able to provide specific and detailed information on the ways in which a person communicates. This information can be used by ''communication partners'' to guide their interactions with a person whom they do not know well. Five samples of experts - parents, researchers, residential workers, speech pathologists, and special education teachers - rated 16 "best practice" indicators and then rated Biala-II in relation to these indicators. They also answered questions about specific features of the profile with attention to the methodology employed and the likelihood that its use would improve communication with people with an intellectual disability. The results reveal a high level of support for the profile.  相似文献   

20.
论高校高素质创造型人才培养的保障体系   总被引:1,自引:0,他引:1  
经济社会的发展呼唤创造型人才。培养高素质创造型人才是高校的责任。而培养高素质创造型人才,必须有高素质创造型的教师队伍;必须形成创造教育教学的氛围与情境;必须构建创造性教育教学模式和培养机制;必须使学生创造性学习;必须有良好的社会条件和机制来支持。  相似文献   

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