共查询到20条相似文献，搜索用时 468 毫秒
1.
利用2,4-二氨基苯酚在铂阳极上的催化氧化和不可逆电对构成的双安培定量分析理论,建立了直接测定2,4-二氨基苯酚的流动注射双安培法。使用已在恒电位下进行过预阳极化处理的双铂电极,在外加电压为零伏特时,通过在阳极上2,4-二氨基苯酚的氧化和在阴极上氧化铂的还原这两个不可逆电极反应过程,构成流动注射双安培检测体系。结果表明,在pH：8．69的B—R缓冲溶液中,2,4-二氨基苯酚的氧化电流与其浓度符合线性关系（r=0．9946,n=10）,其线性范围为4．0×10^-6mol／L～8．0×10^-4mol／L,检出限为6．0×10^-7mol／L。连续36次测定6．0×10^-5moL／L的2,4-二氨基苯酚溶液,电流值的RSD=3．12％。用流动注射双安培法测定样品中2,4-二氨基苯酚的含量,选择性和灵敏度很高,测定结果准确度较高。 相似文献
2.
《淮北师范大学学报》2016,(1)
用循环伏安法扫描聚合和电化学还原石墨烯,制备聚L-苯丙氨酸/还原石墨烯修饰电极,该电极对对乙酰氨基苯酚具有较好的催化能力和较快的电子传递速率.利用循环伏安法和差分脉冲伏安法探究对乙酰氨基苯酚在该电极上的电化学行为,对乙酰氨基苯酚在电极表面的氧化还原过程受扩散控制.在最佳实验条件下,对乙酰氨基苯酚在0.610 V处产生一个氧化峰.采用差分脉冲法测定对乙酰氨基苯酚的线性范围为5.00×10-7~2.50×10-4mol/L,检出限为1.0×10~(-7)mol/L.该法用于测定药物中对乙酰氨基苯酚,结果满意. 相似文献
3.
刘娟 《漯河职业技术学院学报》2010,9(5):1-3
以对氨基苯磺酸、苯酚和甲醛为主要原料,合成出氨基磺酸系高效减水剂（简称AH）。对掺AH的水泥净浆流动度进行测定,得出了合成工艺优化条件：摩尔比为n（对氨基苯磺酸）：n（苯酚）=1：2-2.5,n（对氨基苯磺酸＋苯酚）：n（甲醛）=1：1.15-1.3;反应pH值7-10;反应温度75℃-95℃;反应物浓度35%;反应时间5h左右,此条件下的产物分散性能最佳。通过对优化工艺下合成的AH的红外谱图进行分析,表明AH是含有减水基团-SO3H、-OH和-NH2的理想高效减水剂。 相似文献
4.
《中学生数理化(高中版)》2016,(9)
<正>氨基酸是羧酸分子中烃基上的氢原子被氨基(—NH_2)取代的化合物。氨基酸分子里既有氨基(—NH_2)又有羧基(—COOH),属于取代羧酸。组成蛋白质的氨基酸几乎都是α-氨基酸,即氨基在羧基的α位上。—COOH的邻位碳原子称为α-碳原子,该原子上的氢原子称为α-H,氨基称 相似文献
5.
2—水杨醛缩氨基苯酚·氨合镍（II）三元配合物的合成与表征 总被引：1，自引：0，他引：1
介绍了2-水杨醛缩氨基苯酚·氨合镍(II)三元配合物的合成,通过元素分析,红外、摩尔电导、紫外、热重-差热、磁化率等对其进行了表征。结果表明2-水杨醛缩氨基苯酚·氨合镍(II)形成1:1:1型的平面四方形结构的中性配合物。 相似文献
6.
高健 《连云港职业技术学院学报》2005,18(2):54-56
通过2-[二（2-氨基乙基）氨基]乙醇和2，6-二甲酰基-4-R-苯酚钠的Sehiff Base缩合反应得到了系列带羟乙基手臂的六氮杂双核Cd（Ⅱ）环合物，利用元素分析、红外光谱、摩尔电导、电喷雾质谱等分析手段对产物进行了表征和研究。 相似文献
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以变色酸为母体设计合成了对羧基偶氮羧碘显色剂，磺酸基是该显色剂的功能团，从对氨基苯甲酸出发，进行磺化，得2—氨基—5—羧基苯磺酸．将它重氮化。与变色酸二钠盐偶联．得偶氮羧磺I，再以偶氮羧磺I为母体．与对氨基苯酸偶联，得对羧基偶氮羧磺。 相似文献
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<正> 例1 人体免疫球蛋白中,1gG(一种免疫球蛋白)由4条肽链构成,共有764个氨基酸,则该蛋白质分子中至少含有游离氨基和羧基数分别是A.764和764 B.760和760C.762和762 D.4和4解析该题应强调对“至少”和“游离”二词的理解。一个氨基酸分子“至少”有一个氨基和一个羧基,R 基中是否有氨基和羧基不予考虑。不参与脱水缩合的氨基和羧基方可称为“游离”的氨基和羧基,参与了脱水缩合的氨基和羧基不可称为“游离”的氨基和羧基。如此,n 个氨基酸(至少有 n 个氨基和 n个羧基)脱水缩合形成一条多肽链时,形成 n-1个肽键,脱掉n-1个水分子,用掉 n-1个氨基和 n-1个羧基,剩余1个氨基和1个羧基,故1条多肽链至少含有1个游离的氨基和1 相似文献
11.
罗艳萍 《读与写:教育教学刊》2008,5(6)
The communication of people partially is the communication of cultures. Culture has a direct effect on international commercial activities in all aspects. Different conceptions about time, space, equality, law and the like, lead people to deal with things in different ways. So to know cultures of the counterpart is to facil-itate our enterprises so as to have a smooth and successful communication in commercial activity. 相似文献
12.
Richard Denner 《海外英语》2007,(4):14-15
Rosco and I wait for the fishermen to return.I sit at a wooden bench near the store at Mt.Baker Resort and watch the clouds change shape. Rosco has my belt around his neck and an eight foot tow chain hooked to a tree. Dogs must be on a leash. Ducks and rabbits are loose. 相似文献
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Given a graph G,a subgraph C is called a clique of G if C is a complete subgraph of G maximal under inclusion and |C|≥2. A clique-transversal set S of G is a set of vertices of G such that S meets all cliques of G. The clique-transversal number, denoted as TC (G), is the minimum cardinality of a clique-transversal set in G. The clique-graph of G, denoted as K (G), is the graph obtained by taking the cliques of G as vertices, and two vertices are adjacent if and only if the corresponding cliques in G have nonempty intersection. Let F be a class of graphs G such that F={G|K(G) is a tree}. In this paper the graphs in F having independent clique-transversal sets are shown and thus TC (G)/|G|≤1/2 for all G ∈ F. 相似文献
14.
邱崇丙 《唐山师范学院学报》2014,(1):21-23
汉字的六书,《说文》对“转注”一类,语焉不详。后世学者提及转注,也仅限于许慎所举出的例字。《汉字例说》一文,作者从转注的角度综合考虑,对部分现代常用字作了分析,跟传统的解释有所不同。希望能抛砖引玉,互相切磋,以推进学术研究。 相似文献
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陈美曦 《山东教育学院学报》2008,23(2):103-107
Different nations have different social cultures, and the social culture of every nation is developing with the development of the nation, language is greatly influenced by social culture, which enables language to possess national and historical characteristics. Word is the smallest, independent, meaningful linguistic unit of language. It can well reflect the national and historical characteristics. From synchronic aspect, the social and cultural influence on word meaning is mainly embodied in conceptual and associative meanings of word. The incorrespondence of word meaning is a phenomenon that exists in both conceptual and associative meanings of word among different languages. From diachronic aspect, the development of social culture causes some changes of word meaning to some extent. Therefore, social culture plays a key role in vocabulary learning and mastery of a language. 相似文献
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Rachel Zupek 《海外英语》2007,(11):40-41
我们绝大部分人都同意一件事情——我们喜欢金钱。但是你对金钱的喜欢之情足够到让你创立一份事业么?.财富通常被人忽视,主要在于人们不能真正了 相似文献
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《海外英语》2007,(4):36
There are numbers of crossroads on our long and unpredictable life journey where we totally have no idea about which direction to choose. No matter what our decision is, we should not turn back, but face the music and go ahead instead. I am this kind of girl who always does try without regretting, one example is how I dealt with my love. 相似文献
19.
YANGShiguo 《重庆大学学报(英文版)》2004,3(1):86-88
The problem on the geometrc inequalities involving an n-dimensional simplex and its inscribed simplex is studied. Aninequality is established, which reveals that the difference between the squared circumradius of the n-dimensional simplex andthe squared distance between its circumcenter and barycenter times the squared circumradius of its inscribed simplex is not lessthan the 2(n-1)th power of n times its squared inradius, and is equal to when the simplex is regular and its inscribed siplex is atangent point one. Deduction from this inequality reaches a generalization of n-dimensional Euler inequality indicating that thecircumradius of the simplex is not less than the n-fold inradius. Another inequality is derived to present the relationship betweenthe circumradius of the n-dimensional simplex and the circumradius and inradius of its pedal simplex. 相似文献
20.
Migration occurs behind a variety of reasons and has a great effect on the whole world. People may migrate in order to improve their economic situation, or in order to escape civil strife, persecution, and environmental disasters. The impact of migration is complex, bringing both benefits anddisadvantages. This paper briefly talks about the causes of migration, the allocation of benefits, and the ways in which individual countries and the international community deal with this important subject. 相似文献