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1.
Single crystal Ga x In1−x As films have grown up on GaAs(100) substrate at 375°C and on InP(100) substrate at 390°C, respectively, by the method of rf-sputtering with using undoped GalnAs polycrystal as target. However, on Si(100) or Si(111) substrates at 260–390°C, even at 465°C, only polycrystalline films were obtained. In addition, the structure, composition, electrical characteristic and optical properties of the Ga x In1−x As films were investigated using X-ray diffraction (XRD), reflection of high energy electron diffraction (RHEED), energy dispersion analyzer of X-ray (EDAX), Hall measurements and spectroscopic ellipsometry.  相似文献   

2.
INTRODUCTION The physics of plastic deformation and crack propagation at atomic level is complex but is essential for the development of new materials. This requires an understanding of the atomic level phenomena associated with the plastic deformation. In this con- text, emission of electromagnetic radiation (EMR) during plastic deformation and crack propagation in metals and alloys, and generation of transient mag- netic fields during crack initiation in ferromagnetic materials are rep…  相似文献   

3.
Ａｌｕｍｉｎｕｍ ＡｌｌｏｙｓTX１ＩｎｔｒｏｄｕｃｔｉｏｎＦｅ－Ａｌｉｎｔｅｒｍｅｔａｌｉｃｓｈａｖｅｇｒｅａｔｐｏｔｅｎｔｉａｌｉｔｉｅｓｆｏｒｓｔｒｕｃｔｕｒａｌａｐｐｌｉｃａｔｉｏｎｓｏｗｉｎｇｔｏｔｈｅｉｒｇｏｏｄｍｅｃｈａｎｉｃａｌｐｒｏｐ...  相似文献   

4.
Nanometer-sized SnO2 particles were prepared by a sol-gel method using inorganic salt as a precursor material. Its crystallization was investigated by means of TG-DTA, IR absorption spectra, X-ray diffractometry and TEM as well as its resistivity change and the gas sensitivity varied with temperature were measured in various reducing gas. The results indicate that well-crystallized nano-sized SnO2 with size around 15nm can be obtained at annealing temperature 600°C. The activation energy for the growth of nano-SnO2 was calculated to be 26. 55kJ. mol−1 when the annealing temperature was higher than 500°C. The measurements also show that there is a peculiar resistance change varied with temperature for nano-SnO2. It has relevance to the increase in surface adsorbed oxygen. The selective detectivities to C4H10 and petrol can be increased when ruthenium ion was doped in nano-SnO2 as a catalyst and so do the gas sensitivity to CO, CH4, H2 etc. when rhodium ion was doped in. The detection to the several reducing gas can be realized when the temperature ranged from 260°C to 400°C.  相似文献   

5.
The yeast strain （Y18） was isolated from a soil sample collected from Fildes Peninsula, Antarctica. The strain is a psychrophilic yeast with optimum and maximum growth temperatures of 10 ℃ and 18 ℃, respectively. Teliospores were formed after 7 d on malt agar, when the germination of teliospores was observed. Both inositol and D-glucuronate were assimilated. Positive results of the DBB （diazonium blue B） color reaction, urease test, and starch formation were observed. The major CoQ is Qs. All results indicated that Y18 belongs to the genes of Mrakia. The 18S rDNA sequence analyses showed that Y18 is closely related to Mrakiafrigida. DNA-DNA relatedness study, and some biochemistry characteristics indicated that Y18 represents a new species for which Mrakia psychrophila sp. nov. is proposed.  相似文献   

6.
Silicon carbide (SiC) composites were prepared by hot-press sintering from α-SiC starting powders with BaAl2Si2O8 (BAS). The effects of additives on densification, microstructure, flexural strength, and fracture behavior of the liquid phase sintered (LPS) SiC composites were investigated. The results show that the served BAS effectively promotes the densification of SiC composites. The flexural strength and fracture toughness of the SiC composites can reach a maximum value of 454 MPa and 5.1 MPa·m1/2, respectively, for 40% (w/w) BAS/SiC composites. SiC grain pullout, crack deflection, and crack bridging were main toughening mechanisms for the sintered composites.  相似文献   

7.
Hydroxyapatite bioceramics is simulated by using finite element method (FEM).The influences of porosity,hole shape,angle of crack and other parameters on the ceramics are analyzed.The results show that with the increase of the angle between crack and horizontal direction,the stress intensity factor KⅠdecreases gradually,but stress intensity factor K II increases at first and then it decreases.The value of K Ⅱ reaches maximum when the angle between crack and horizontal direction is 45°.KⅠ and K Ⅱ rise with the increase of porosity,and they are almost the same for the circular and hexagonal holes.For elliptical holes,KⅠand KⅡreach maximum when the long axis of ellipse is perpendicular to the loading direction and they reach minimum when the same axis is parallel to the loading direction.Moreover,with the increase of the angle between the long axis and loading direction,KⅠ and KⅡ increase gradually.  相似文献   

8.
Ethene/norbornene copolymerization by the catalyst system [Me2Si(3-tertBuCp)(NtertBu)]TiCl2/MAO was investigated in detail at 30 °C, 60 °C, and 90 °C. A mass flow controller was used in this work to obtain kinetic data and investigate temperature's effects on activity, norbornene incorporation, copolymerization parameter, microstructure, glass transition temperature, and molar masses were described. High copolymerization valuesr ξ and high alternation are determined. The number of isotactic alternating sequences is much higher than that of the syndiotactic alternating sequences.  相似文献   

9.
Transgenic Brassica compestris L.spp.chinensis plants expressing a choline oxidase(codA) gene from Arthrobacter globiformis were obtained through Agrobacterium tumefaciens-mediated transformation.In the transgenic plants,codA gene expression and its product transportation to chloroplasts were detected by the enzyme-linked immunosorbent assay(ELISA) examination,immunogold localization,and 1 H-nuclear magnetic resonance( 1 H-NMR) . Stress tolerance was evaluated in the T3 plants under extreme temperature and salinity conditions.The plants of transgenic line 1(L1) showed significantly higher net photosynthetic rate(Pn) and Pn recovery rate under high(45°C,4 h) and low temperature(1°C,48 h) treatments,and higher photosynthetic rate under high salinity conditions(100,200,and 300 mmol/L NaCl,respectively) than the wild-type plants.The enhanced tolerance to high temperature and high salinity stresses in transgenic plants is associated with the accumulation of betaine,which is not found in the wild-type plants.Our results indicate that the introduction of codA gene from Arthrobacter globiformis into Brassica compestris L.spp.chinensis could be a potential strategy for improving the plant tolerance to multiple stresses.  相似文献   

10.
To investigate the influence of microwave radiation on the human fibroblast nuclei, the effects of three variants of electromagnetic wave polarization, linear and left-handed and right-handed elliptically polarized, were examined. Experimental conditions were: frequency (f) 36.65 GHz, power density (P) at the surface of exposed object 1, 10, 30, and 100 μW/cm2, exposure time 10 s. Human fibroblasts growing in a monolayer on a cover slide were exposed to microwave electromagnetic radiation. The layer of medium that covered cells during microwave exposure was about 1 mm thick. Cells were stained immediately after irradiation by 2% (w/v) orcein solution in 45% (w/v) acetic acid. Experiments were made at room temperature (25 °C), and control cell samples were processed in the same conditions. We assessed heterochromatin granule quantity (HGQ) at 600× magnification. Microwave irradiation at the intensity of 1 μW/cm2 produced no effect, and irradiation at the intensities of 10 and 100 μW/cm2 induced an increase in HGQ. More intense irradiation induced more chromatin condensation. The right-handed elliptically polarized radiation revealed more biological activity than the left-handed polarized one.  相似文献   

11.
In this paper, crude monkshood polysaccharide was isolated from Radix Aconiti Lateralis Preparata. The effects of crude monkshood polysaccharide on Escherichia coli and Staphylococcus aureus were investigated by microcalorimetry. The power-time curves of the bacterial growth at various concentrations (c) of crude monkshood polysaccharide were plotted with a TAM air isothermal microcalorimeter at 37 °C. The growth rate constant (μ), inhibitory ratio (I), peak-height (P m), and peak-time (t m) were calculated. From the data, the relationship between μ and c also was established. The growth rate constant μ decreased with the increasing concentrations of crude monkshood polysaccharide. Moreover, P m reduced and t m increased with increasing concentrations. The experimental results revealed that crude monkshood polysaccharide had inhibitory activity towards S. aureus and E. coli. Results obtained from our study strongly suggest that microcalorimetry is a fast, simple, and more sensitive technology that can be easily performed to study the effect of drugs on bacteria.  相似文献   

12.
INTRODUCTION Enzymes are efficient and specific biocatalysts widely used in food industries, but their application in industrial process often involves special properties not found in natural source enzymes. In order to ob- tain desirable enzymes, in the past ten years, scientists have developed rational (Kurth et al., 1998; Mouratou et al., 1999; DeSantis et al., 1999) and irrational de- sign methods (Babbitt and Gerlt, 1997; O’Brien and Herschlag, 1999) to improve the enzyme propert…  相似文献   

13.
The production of elastase by Bacillus sp. EL31410 at various temperatures was investigated. In order to study the effect of temperature on elastase fermentation, different cultivation temperatures, ranging from 39 °C to 28 °C, were evaluated in shake flask. The result indicated that 37 °C was best for cell growth at earlier stage; while maximum elastase activity was obtained when the cells were cultivated at 30 °C. This result was verified by batch fermentation in 5-L bioreactor under 37 °C and 30 °C temperature, respectively. The specific cell growth rate at 37 °C was higher than that at 30 °C during earlier stage of cultivation. The maximum value [5.5 U/(h·g DCW)] of elastase formation rate occurred at 24 h at 30 °C compared to 4.6 U/(h·g DCW) at 30 h at 37 °C. Based on these results, two-stage temperature shift strategy and oscillatory temperature cultivation mode were evaluated in the next study. When compared to single temperature of 37 °C or 30 °C, both two-stage temperature shift strategy and oscillatory temperature strategy improved biomass but did not yield the same result as expected for elastase production. The maximum biomass (both 8.6 g/L) was achieved at 30 h at 37 °C, but at 42 h using two-stage temperature cultivation strategy. The highest elastase production (652 U/ml) was observed at 30 °C in batch process. It was concluded that cultivation at constant temperature of 30 °C was appropriate for elastase production by Bacillus sp. EL31410. Project (No. 20276064) supported by the National Natural Science Foundation of China  相似文献   

14.
Objective: To determine the range of body temperature in a group of healthy Chinese term neonates over the first 72 hours of life and to assess the influence of body weight, gestational age and route of delivery. Method: All 200 consecutive cases of neonates delivered at our hospital from March to August 2001 were included in this retrospective study. Temperatures were measured immediately after delivery, after 30 minutes, 1 hour, 2 hours, 8 hours and 15 hours and on the 2nd and 3rd day. Axillary temperatures ranging from 36.5 oC to 37 oC were regarded as normal. No cases of maternal fever or systemic infection of the newborns were discovered. All infants were discharged in good general condition. Results: The mean rectal temperature at birth was 37.19 ℃. The lowest average temperature was reached at 1 hour after delivery (36.54 ℃) with a significant difference between natural delivery (36.48 ℃) and section (36.59 ℃) (P<0.05). Temperature subsequently rose to 36.70 ℃ at 8 hours and 36.78 ℃ at 15 hours (P<0.05). Hypothermia was seen in 51.8% and hypothermia in 42.5% of the patients. On the 3rd day after delivery, 96% of all temperatures were in the normal range. A significant relation was found between hypothermia and both low birth weight (P<0.001) and low gestational age (P<0.05). Conclusion: The reference range presently used did not include all physiological temperatures in the first 72 hours of life. Considering other factors, such as birth weight, route of delivery, gestational age and body temperature on the 2nd and 3rd day of life, may help to correctly assess the significance of temperatures beyond the reference range.  相似文献   

15.
<正>Porous Si3N4 self-reinforce ceramics were prepared by gelcasting using agarose solutions. By changing the agarose content in the slurries, the porous silicon nitride ceramics with different porosities, α→β-Si3N4 phase transformation, and mechanical properties were obtained. When the agarose content changed from 0.2% to 0.8% (w/w, based on powder), the porosities increased from 10.3% to 21.4%, while the fracture strength decreased from 455 to 316 MPa and the fracture toughness decreased from 6.6 to 5.5 MPa·m1/2. Many fibrous β-Si3N4 grains grown from the internal wall of the round pores is the typical microstructure of the gelcasting porous silicon nitride ceramic. Both elongated β-Si3N4 grains and suitable interfacial bonding strength contributes to high fracture toughness by favoring crack deflection and bridging. The growth mechanisms of fibrous grains resulted from the synergy of solution-diffusion-reprecipitation and vapor-liquid-solid (VLS).  相似文献   

16.
Sweetpotato starch thermal properties and its noodle quality were analyzed using a rapid predictive method based on near-infrared spectroscopy （NIRS）. This method was established based on a total of 93 sweetpotato genotypes with diverse genetic background. Starch samples were scanned by NIRS and analyzed for quality properties by reference methods. Results of statistical modelling indicated that NIRS was reasonably accurate in predicting gelatinization onset temperature （To） （standard error of prediction SEP=2.014 ℃, coefficient of determination RSQ=0.85）, gelatinization peak temperature （Tp） （SEP=-1.371 ℃, RSQ=0.89）, gelatinization temperature range （Tr） （SEP=2.234 ℃, RSQ=0.86）, and cooling resistance （CR） （SEP=0.528, RSQ=0.89）. Gelatinization completion temperature （To）, enthalpy of gelatinization （△H）, cooling loss （CL） and swelling degree （SWD）, were modelled less well with RSQ between 0.63 and 0.84. The present results suggested that the NIRS based method was sufficiently accurate and practical for routine analysis of sweetpotato starch and its noodle quality.  相似文献   

17.
TiO2 fibers were prepared via alternatively introducing water vapor and Ti precursor carried by N2 to an APCVD （chemical vapor deposition under atmospheric pressure） reactor at ≤200 ℃. Activated carbon fibers （ACFs） were used as templates for deposition and later removed by calcinations. The obtained catalysts were characterized by scanning electron micros- copy （SEM）, transmission electron microscopy （TEM）, Brunauer, Emmett and Teller （BET） and X-ray diffraction （XRD） analysis The pores within TiO2 fibers included micro-range and meso-range, e.g., 7 nm, and the specific surface areas for TiO2 fibers were 141 m^2/g and 148 m^2/g for samples deposited at 100 ℃ and 200℃ （using ACFI700 as template）, respectively. The deposition temperature significantly influenced TiO2 morphology. The special advantages of this technique for preparing porous nano-material include no consumption of organic solvent in the process and easy control of deposition conditions and speeds.  相似文献   

18.
A new concept of low-cost direct air capture technology integrated with a fertilization system is proposed, as an alternative to the application of air derived CO2. A moisture swing sorbent can elevate the CO2 concentration from 400 parts per million (ppm) to several thousand ppm, and this can be used to cultivate plants. Desorption isotherms were determined and are described well by a Langmuir model. The adsorption rate constant and the desorption rate constant were gained at 25 °C, 35 °C, and 45 °C under 1000 ppm concentration of CO2. In accelerated cultivation experiments, the effects of CO2 concentration, light intensity, and spectrum on the CO2 uptake rate of the plants were investigated. A multi-bed desorption system which is capable of providing a continuous and stable CO2 supply for a greenhouse is demonstrated based on the desorption characteristic and CO2 uptake feature of plants. An energy and cost assessment for the integrated system was performed and the results indicated that minimum energy requirements and cost estimate of CO2 are 35.67 kJ/mol and 34.68 USD/t, respectively. This makes direct air capture a competitive and sustainable carbon source for agriculture.  相似文献   

19.
The objectives of this study are: (a) Evaluate science major freshman students’ ability to differentiate between heat energy and temperature, after having studied the topic of thermochemistry; (b) ascertain the degree to which students resist change from the caloric to the kinetic-molecular theory; (c) study the ability to differentiate between heat energy and temperature and its relationship to solving a problem of thermochemistry. Science major freshman students (n = 76) were tested on a three-item Test of Heat Energy and Temperature (THT) and a Thermochemistry Problem (TP). Both THT and the TP formed part of a semester exam given after the topic of thermochemistry had been studied in class. Results obtained show that even after having studied thermochemistry in an introductory freshman course, students have considerable difficulty in differentiating between heat energy and temperature. Although, all three items of THT required the understanding of kinetic-molecular theory, percentage of correct responses varied considerably: Item 1 (72%), Item 2 (64%), and Item 3 (51%). A correct response on Item 3 meant that different amounts of water in two different vessels at 100 °C, would have the same average kinetic energy, but the heat energy required to attain 100 °C was different—hence the confusion with heat as a substance (caloric theory). It was found that students who had good conceptual understanding on the TP did not perform significantly (χ 2 = 0.023) better on the THT. It is concluded that as science teachers we must be aware of the difficulties associated with the differentiation between heat energy and temperature and hence the need for teaching thermochemistry in order to facilitate conceptual understanding.  相似文献   

20.
(K0.47Na0.47Li0.06)NbO3 (KNLN) lead-free ceramics were prepared by molten salt synthesis (MSS) method using k2CO3-Na2CO3 eutectic mixtures as the flux. The microstructure and piezoelectric properties when sintered at 980-1 030 ℃ were investigated. The calcined powders were examined by X-ray diffraction. The microstructure of the calcined powders and sintered bodies was observed using a scanning electron microscope (SEM).The piezoelectric constant d33 was measured using a quasi-static piezoelectric d33 meter. The planar coupling coefficient Kp was calculated by resonance-antiresonance method. The experimental data for each sample's performance indicators were the average values of 8 specimens. The relative densities of sintered specimens are above 97%, and the dielectric loss is below 0.03. It was found that (K0.47Na0.47Li0.06)NbO3 prepared by MSS is compact and lead-free. The piezoelectric constant d33 is 216 pC·N-1 and the planar electromechanical coupling factor Kp is 0.352.  相似文献   

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