多孔陶瓷管式露点间接蒸发冷却器的设计计算     

毛秀明  黄翔  文力 《东南大学学报》2010,26(2):205-208

为了提高管式间接蒸发冷却器壁面的亲水性,提出了一种采用多孔陶瓷材料的新方法.该方法将多孔陶瓷材料与蒸发冷却技术有机结合,从一次空气风量和二次空气风量、一次空气状态参数和二次空气状态参数、冷却器结构、固体多孔陶瓷管的传热以及冷却器阻力等方面对多孔陶瓷管式露点间接蒸发冷却器进行了设计计算.计算结果表明该设计合理可行.最后,依据设计制作出多孔陶瓷管式露点间接蒸发冷却器.  相似文献   

脉冲激光沉积法在多孔硅衬底上制备ZnS薄膜     

王彩凤  胡波  李清山 《滨州学院学报》2010,26(6)

用电化学阳极氧化法制备了一定孔隙率的多孔硅样品,然后用脉冲激光沉积法以PS为衬底生长一层ZnS薄膜.用X射线衍射仪、扫描电子显微镜和荧光分光光度计分别表征了ZnS薄膜的结构、形貌和ZnS/PS复合膜的光致发光性质.XRD结果表明,制备的ZnS薄膜沿β-ZnS(111)方向择优生长,结晶质量良好,但衍射峰的半峰全宽较大;SEM图像显示,ZnS薄膜表面出现一些凹坑,这是衬底PS的表面粗糙所致.室温下的光致发光谱表明,沉积ZnS薄膜后,PS的发光峰蓝移.把ZnS的蓝绿光与PS的橙红光叠加,在可见光区450~700 nm形成了一个较宽的光致发光谱带,ZnS/PS复合膜呈现较强的白光发射.  相似文献   

硅藻土为模板糠醇为碳源制备多孔炭     

刘贵阳  郭俊明  王海军  李新明  王宝森  何英 《蒙自师范高等专科学校学报》2010,8(2):5-6,15

以天然硅藻土为模板,糠醇为碳源,通过模板法能制备了多孔炭材料.N2吸附研究表明,此多孔炭的比表面积为542m2/g,中孔率可达54.7%,是一种既有微孔,同时也富含中大孔的多孔材料.  相似文献   

High density porous polyethylene material （Medpor） as an unwrapped orbital implant   总被引：1，自引：1，他引：0  

Chen YH  Cui HG 《Journal of Zhejiang University. Science. B》2006,7(8):679-682

Objective： To introduce the clinical effect among patients who received an unwrapped orbital implant with high density porous polyethylene material （Medpor） after enucleation or evisceration. Methods： Retrospective analysis of a series of 302 patients with anophthalmia who underwent placement of an unwrapped high density porous polyethylene orbital implant. We compared the patients （n=180） who accepted primary implant placement with those （n=122） who accepted secondary implant placement. Parameters evaluated included： age at time of surgery, date of surgery, sex, implant type and size, surgery type, the surgical procedure and technique performed, and complications. Results： The time of follow-up ranged from 2.0 to 58.0 months （mean 32.5 months）. A total of 5 of 302 （1.66%） cases had documented postoperative complications. The following problems were noted after surgery： implant exposure, 3 patients （0.99%）; implant removed due to orbital infection, 1 patient （0.34%）; ptosis, 1 patient （0.34%）. There were no significant complications＇observed in other 297 cases and all implants showed good orbital motility. The clinical effect of primary implant placement is better than that of secondary placement. Conclusion： High density porous polyethylene material can be used successfully as an unwrapped orbital implant in anopthalmic socket surgery with minimal complications. The material is well tolerated, nonantigenic and has low rate of infection and migration.  相似文献   

具有规则阵列结构的阳极氧化铝模板的制备     

李明 《玉溪师范学院学报》2007,23(8):42-45

用两步阳极过程,分别在硫酸和草酸体系中制备出了纳米孔阵列氧化铝模板.从对其表面进行AFM和SEM表征的结果看,所制备的氧化铝模板微孔排列整齐,局部高度有序.  相似文献   

组合式吸液芯内金属钠固-液相变的数值模拟(英文)     

于萍  张红  许辉  沈妍 《东南大学学报》2014,(4)

采用有限容积法和焓-多孔介质模型数值模拟了组合式吸液芯内金属钠熔化的固-液相变过程.由于液态金属钠和组合式吸液芯的导热系数在同一数量级,因而采用单温度模型,模拟过程中考虑了非达西效应影响和液态金属钠的自然对流现象.研究结果发现,组合式吸液芯中金属纤维毡厚度越小,金属钠受热熔化的速度越快,且熔化后的液态钠流速达到最大值所用的时间越短,进而可以缩短热管启动时间;组合式吸液芯中金属纤维毡厚度越大,竖直加热壁面的温度分布越均匀、壁面温差越小,进而减少了加热壁面产生过热点的可能.  相似文献   

致孔剂对多孔酚醛树脂微球粒径的影响及热性能分析     

张慕诗 《常熟理工学院学报》2014,(4):66-71

以苯酚、甲醛为单体,水为分散介质,PVA1788为分散剂,甲苯、DOP、十八醇等为致孔剂,在NaOH催化条件下,采用悬浮缩聚法制备了多孔酚醛树脂微球(PF微球).讨论了致孔剂种类及用量对酚醛树脂微球粒径及其分布的影响,测试了甲苯与十八醇配伍制的PF微球的热性能.通过实验发现,在混合致孔剂(甲苯分别于DOP、十八醇配伍)条件下的微球产率较高,粒径均一;甲苯+十八醇致孔剂条件下的PF微球在450℃后才发生较大的热失重,热稳定性能较好.  相似文献   

钛表面制备多孔氧化物陶瓷层的实验设计     

尤德强  王泽  张鹏  李卫 《实验室研究与探索》2013,32(6):18-20

为提高生物医用金属钛材料表面的生物活性和生物相容性,以乙酸钙、β-甘油磷酸钠混合溶液作为电解液,采用微弧氧化实验方法,在金属钛表面制备出具有多孔结构的氧化物陶瓷层。用X射线衍射仪(XRD)、扫描电子显微镜(SEM)以及能谱分析仪(EDS)对氧化物陶瓷层的组成及结构进行了分析。结果表明:氧化物陶瓷层的主晶相为锐钛矿型二氧化钛,同时含有钛、金红石型二氧化钛以及钛酸钙相;试样表面形成大量的微孔,孔径1～3μm,孔洞分布均匀;电解液中的Ca、P元素也参与了反应,并沉积在氧化物陶瓷层内。通过此实验方法可以有效提高金属钛的生物活性和生物相容性。  相似文献   

A partially fluorinated ligand for two super-hydrophobic porous coordination polymers with classic structures and increased porosities     

Chao Wang  Dong-Dong Zhou  You-Wei Gan  Xue-Wen Zhang  Zi-Ming Ye  Jie-Peng Zhang 《国家科学评论(英文版)》2021,8(3)

3-Ethyl-5-trifluoromethyl-1,2,4-triazole is synthesized by a one-pot reaction. Using this asymmetric triazole ligand bearing one trifluoromethyl and one ethyl as side groups, we construct two new porous coordination polymers, MAF-9 and MAF-2F, being isostructural with the classic hydrophobic and flexible materials, FMOF-1 and MAF-2, based on symmetric triazole ligands bearing two trifluoromethyl groups or two ethyl groups, respectively. MAF-9 and MAF-2F can adsorb large amounts of organic solvents but completely exclude water, showing superhydrophobicity with water contact angles of 152^o in between those of FMOF-1 and MAF-2. MAF-9 exhibits very large N₂-induced breathing and colossal positive and negative thermal expansions like FMOF-1, but the lower molecular weight and smaller volume of MAF-9 give 16% and 4% higher gravimetric and volumetric N₂ uptakes, respectively. In contrast, MAF-2F is quite rigid and does not show the inversed temperature-dependent N₂ adsorption and large guest-induced expansion like MAF-2. Further, despite the higher molecular weight and larger volume, MAF-2F possesses 6% and 25% higher gravimetric and volumetric CO₂ uptakes, respectively. These results can be explained by the different pore sizes and side group arrangements in the two classic framework prototypes, which demonstrate the delicate roles of ligand side groups in controlling porosity, surface characteristic and flexibility.  相似文献   

以滇蔗茅为模板合成的Co/SiO₂在环己烷氧化反应中催化性能的影响     

秦云  姚文华 《保山学院学报》2012,(2):20-23

考察以滇蔗茅为模板合成的Co/SiO2催化剂对环己烷催化氧化的性能,探讨了反应时间、反应温度、催化剂用量、溶剂、氧化剂用量等对该催化反应的影响。实验表明,在催化剂用量为50m g;环己烷750m g;以冰醋酸为溶剂,5.0m L 30%的H2O2;反应温度373K;反应时间10h的条件下,环己烷转化率为71.0%,环己酮的选择性为76.7%,环己醇选择性为21.2%。  相似文献