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The effect of CaF2-doped ZrO2 catalyst for the synthesis of dimethyl carbonate (DMC) was studied by X-ray diffraction (XRD), CO2-temperature programmed desorption (TPD), Raman spectra, and X-ray photoelectron spectroscopy (XPS). Catalytic performance was evaluated in the bath and distillation reactors. Results showed that the CaF2/ZrO2 catalysts had activity and stability for DMC synthesis. 相似文献
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Gas chromatography (GC) analysis of sulfer dioxide is challenging because SO2 is a highly mobile and chemically active molecule. For the conventional GC method with flame photometric detector (FPD) and direct-injection, it is often ineffective particularly when the SO2 level is as low as on the trace level. In this paper, a modified GC system integrated with an adsorption-desorption device was developed to detect the trace SO2 impurity in H2 fuel. Adsorbent GDX-502 is used in the adsorber to adsorb/collect SO2 from the sample gas and desorb/release it in a concentrated flow so that the conventional GC at downstream could detect it with an acceptable accuracy. 相似文献
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