| 过渡金属磷硫配体、三苯基膦配合物的合成和表征 |
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| 引用本文： | 邓谦,蔡铁军,张建设,赵转云.过渡金属磷硫配体、三苯基膦配合物的合成和表征[J].湘潭师范学院学报(社会科学版),1995(6). |
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| 作者姓名： | 邓谦 蔡铁军 张建设 赵转云 |
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| 作者单位： | 中科院兰州化学物理所 |
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| 摘 要： | 本文报道在ＴＨＦ和ＣＨ２Ｃｌ２溶液中，用过渡金属三苯基膦氯化物与磷硫配体Ｋｄｔｐ（Ｋ［Ｓ２Ｐ（ＯＥｔ）２］）作用合成了Ｐｄ（ＰＰｈ３）（ｄｔｐ）２·ＴＨＦ等五个配合物．并对这些配合物进行了元素分析、红外光谱、核磁共振谱及质谱等表征。
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| 关 键 词： | 过渡金属 磷硫配体 配合物 |
SYNTHESIS AND CHARACTERIZATION OF TRANSITION METAL COMPLEXES OF SULPHUR PHOSPHOR LIGANDS AND TRIPHENYLPHOSPHINE LIGANDS |
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| Deng Qian, Cai Tiejun, Zang Jianse,Zao Zhuangyun,.SYNTHESIS AND CHARACTERIZATION OF TRANSITION METAL COMPLEXES OF SULPHUR PHOSPHOR LIGANDS AND TRIPHENYLPHOSPHINE LIGANDS[J].Journal of Xiangtan Normal University(Social Science Edition),1995(6). |
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| Authors: | Deng Qian Cai Tiejun Zang Jianse Zao Zhuangyun |
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| Institution: | Deng Qian; Cai Tiejun; Zang Jianse;Zao Zhuangyun; |
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| Abstract: | Five complexes are prepered by reaction of transition metal triphenylphosphine complexes with sulphur phosphor ligands, Kdtp, in the solution of THF and CH2Cl2.The properties of these complexes are characterized by element analysis, IR,NMR,MS,etc |
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| Keywords: | transition metal complex sulphur phosphor Ligands |
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