| 2，4，6—三氯嘧啶的合成 |
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| 引用本文： | 陈时忠.2，4，6—三氯嘧啶的合成[J].科技通报,2001,17(5):57-58. |
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| 作者姓名： | 陈时忠 |
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| 作者单位： | 浙江大学理学院化学系, |
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| 摘 要： | 报道了医药和活性染料中间体2，4，6－三氯嘧啶的合成和鉴定,反应以巴比妥酸为原料，三氯氧磷为氯化剂，反应原料易得，操作简便，产率为87％，产物用红外光谱和核磁共振谱等作了鉴定。
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| 关 键 词： | 2 4 6－三氯嘧啶 巴比妥酸 中间体 合成 鉴定 氧化剂 反应温度 反应产率 |
| 文章编号： | 10017119(2001)05-0057-02 |
| 修稿时间： | 2001年1月16日 |
Synthesis of 2,4,6-Trichloropyrimidine |
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| CHEN,Shi,zhong.Synthesis of 2,4,6-Trichloropyrimidine[J].Bulletin of Science and Technology,2001,17(5):57-58. |
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| Authors: | CHEN Shi zhong |
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| Abstract: | Synthesis and identification of 2,4,6 Trichloropyrimidine were reported in this paper. The method was studied to prepare the title compound by barbituric acid with phosphorus oxychloride. The studied technique had the features of cheap material, simple operation and high yields. The product was analysed by Infra Red spectrum and Nuclear Magnetic Resonance spectrum . |
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| Keywords: | Trichloropyrimidine Barbituric acid Intermediate Synthesis Identification |
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