| 毛细管气相色谱法测定金钱草茎叶中多糖的单糖组成 |
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| 引用本文： | 刘俊劭,江慧华,林志銮,陈培珍.毛细管气相色谱法测定金钱草茎叶中多糖的单糖组成[J].南平师专学报,2011,30(5):48-51. |
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| 作者姓名： | 刘俊劭 江慧华 林志銮 陈培珍 |
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| 作者单位： | 福建省高校绿色化工技术重点实验室,武夷学院环境与建筑工程系,福建武夷山354300 |
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| 基金项目： | 武夷学院校科研基金海西项目(项目编号:xh201002);武夷学院对接南平产业发展科研专项(项目编号:2011DJ10) |
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| 摘 要： | 金钱草多糖经三氟乙酸水解、后利用二甲基亚砜（DMSO）作溶剂，六甲基二硅胺烷（TMDS）和三甲基氯硅烷（TMCS）作硅烷化试剂，将单糖衍生化为三甲基硅醚衍生物，用气相色谱（GC）分析法测定金钱草叶和根茎中多糖的单糖组成。结果表明：金钱草叶和根茎中多糖都是由甘露糖、果糖、核糖、半乳糖、鼠李糖和树胶醛糖单糖组成，其摩尔比分别为1．40：1．00：1．00：4．68：0．98：0．46和1．03：1．00：1．04：1．66：0．56：0．44。
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| 关 键 词： | 金钱草 单糖 毛细管气相色谱法 |
Determination of Monose in the Stems and Leaves of Lysimachia Christinae Hance by Capillary Chromatograph |
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| LIU Junshao JIANG Huihua LIN Zhiluan CHEN Peizhen.Determination of Monose in the Stems and Leaves of Lysimachia Christinae Hance by Capillary Chromatograph[J].Journal of Nanping Teachers College,2011,30(5):48-51. |
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| Authors: | LIU Junshao JIANG Huihua LIN Zhiluan CHEN Peizhen |
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| Institution: | LIU Junshao JIANG Huihua LIN Zhiluan CHEN Peizhen ( Key Laboratory for Green Chemical Engineering Technology of Fujian Higher Education Department of Environmental and Architectural Engineering,Wuyi University,Fujian 354300 ) |
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| Abstract: | Polysaccharide of Lysimachia christinae Hance is hydrolyzed by trifluoroacetic acid. The hydrolysate was derived into trimethylsilylethers derivative with hexamethyedisilane (HMDS) and trimethylchlorosilane (TMCS) as silanizing agent, and dimethyl sulfoxide (DMSO) as solvent .The monosaccharide was determined by GC with capillary column. The results showed that the polysaccharide of leaves and stems were composed of mannose, fructose, ribose, galactose, rhamnose and arabinose, and the molar ratio of those m... |
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| Keywords: | lysimachia christinae hance monose capillary chromatograph |
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