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| 赭石的不同煎出液中Fe2+、Fe3+含量测定研究 | |
| 引用本文： | 康莲薇,熊南燕,李树鱼,肖红赞.赭石的不同煎出液中Fe2+、Fe3+含量测定研究[J].实验技术与管理,2011,28(3):36-38,44. |
| 作者姓名： | 康莲薇 熊南燕 李树鱼 肖红赞 |
| 作者单位： | 1. 河北工程大学理学院,河北,邯郸,056001 2. 河北工程大学医学院,河北,邯郸056002 3. 涉县人民第一医院儿科,河北,涉县,056000 |
| 基金项目： | 河北省教育厅2006年科学研究计划项目 |
| 摘 要： | 目的:建立赭石的水煎液和醋煎液中Fe2+、Fe3+含量分别测定的方法。方法:在pH值为3~5之间,波长为396 nm,以邻二氮菲作显色剂,用紫外-可见分光光度计测定铁含量;在波长为510 nm处测定Fe2+的含量;再由2个浓度之差求得Fe3+的含量。结果:赭石的醋煎液和水煎液中铁含量有明显不同。结论:该方法精度好,回收率大于90%,操作简便,可用于Fe2+、Fe3+含量的测定。 |
| 关 键 词： | 赭石 Fe2+ Fe3+ 邻二氮菲 紫外-可见分光光度法 |
Determining Fe2+,Fe3+contents in ochers decocting different solution |
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| Kang Lianwei,Xiong Nanyan,Li Shuyu,Xiao Hongzan.Determining Fe2+,Fe3+contents in ochers decocting different solution[J].Experimental Technology and Management,2011,28(3):36-38,44. | |
| Authors: | Kang Lianwei Xiong Nanyan Li Shuyu Xiao Hongzan |
| Institution: | 1(1.College of Science,Hebei University of Engineering,Handan 056001,China;2.School of Medicine,Hebei University of Engineering,Handan 056002,China;3.First Hospital,Shexian People of Pediatrics,Shexian 056000,China) |
| Abstract: | AIM: Establishing the separately determining method of the Fe2+,Fe3+ contents in ocher’s the water and the vinegar fries fluid.METHODS: Determining the content of iron by UV-vis spectroscopy,pH3~5,wavelength 396nm,O-phenanthroline as chromogenic reagent;the content of Fe2+ by UV-vis spectroscopy,wavelength 510 nm to obtain the contents of Fe3+ by concentration difference.RESULTS: It is different to the contents of Fe2+,Fe3+in ocher’s water and vinegar fries fluid.CONCLUSION:It can be used for Fe2+,Fe3+ contents which were determined by good precision,recovery rate more than 90% and easy operation. |
| Keywords: | Fe2+ Fe3+ |
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