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微乳液法制备纳米钴蓝颜料及粒径控制
引用本文:杨桂琴,韩冰,王雪松,严乐美,王秀宇.微乳液法制备纳米钴蓝颜料及粒径控制[J].天津大学学报(英文版),2002,8(4).
作者姓名:杨桂琴  韩冰  王雪松  严乐美  王秀宇
作者单位:天津大学理学院,天津,300072
摘    要:利用动态光散射 (DLS)法 ,研究了纳米钴蓝颜料微乳液制备过程中 ,增溶水量对微乳液滴的影响 ,并讨论了微乳液滴对最终制得的粒子粒径的影响 .结果表明 ,调节增溶水量可控制纳米粒子的粒径大小 .对制得的纳米钴蓝颜料进行了XRD和TEM表征 ,并通过颜色测定与分析 ,探讨了纳米粒子的量子尺寸效应 .

关 键 词:微乳液  动态光散射  钴蓝颜料  纳米粒子粒径  量子尺寸效应

Synthesis of Nanometer Cobalt Blue Pigment by Microemulsion Method and Control of Diameter of Particle
YANG Gui-qin,HAN Bing,WANG Xue-song,YAN Le-mei,WANG Xiu-yu.Synthesis of Nanometer Cobalt Blue Pigment by Microemulsion Method and Control of Diameter of Particle[J].Transactions of Tianjin University,2002,8(4).
Authors:YANG Gui-qin  HAN Bing  WANG Xue-song  YAN Le-mei  WANG Xiu-yu
Abstract:The nanometer cobalt blue pigments were prepared by microemulsion method. Using dynamic light scattering(DLS) test method, the influences of water content on the size of liquid drop of microemulsion and the liquid drop of microemulsion on the final diameter of nanometer particle were studied in the course of preparation. Accordingly, the method to control the diameter of nanometer particle by changing water content was established. The nanometer cobalt blue particles were confirmed by XRD and TEM. Color parameters of pigments were determined. The quantum size effect of the pigments was discussed.
Keywords:microemulsion  dynamic light scattering  cobalt blue pigment  diameter of nanometer particle  quantum size effect
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