| 2-氯代苯并噻唑的合成方法研究 |
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| 引用本文： | 刘玉玲,卓馨,朱军.2-氯代苯并噻唑的合成方法研究[J].石家庄学院学报,2013(6):22-24. |
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| 作者姓名： | 刘玉玲 卓馨 朱军 |
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| 作者单位： | 宿州学院自旋电子与纳米材料安徽省重点实验室,安徽宿州234000 |
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| 基金项目： | 宿州学院科研平台开放课题（2011YKF04）;宿州学院一般项目（201lyybl4） |
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| 摘 要： | 研究了以2-巯基苯并噻唑为原料,采用氯甲酸三氯甲酯为氯化剂合成2-氯代苯并噻唑的方法,重点考察了不同溶剂和反应温度对合成反应的影响,提出了合成2-氯代苯并噻唑的一种新方法.
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| 关 键 词： | 2-氯代苯并噻唑 2-巯基苯并噻唑 合成 氯甲酸三氯甲酯 |
A Study of Synthesis of 2-Chlorobenzolthiazole |
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| LIU Yu-ling,ZHUO Xin,ZHU Jun.A Study of Synthesis of 2-Chlorobenzolthiazole[J].Journal of Shijiazhuang University,2013(6):22-24. |
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| Authors: | LIU Yu-ling ZHUO Xin ZHU Jun |
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| Institution: | (Anhui Key Laboratory of Spin Electron ＆ Nanomaterials ,Suzhou University, Suzhou, Anhui 234000, China) |
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| Abstract: | Based on 2-mercaptobenzothiazole as raw material,the synthesis of 2-chlorobenzothiazole is studied with hrichloromethyl-chlorofor-mate. The effect of different solvents and temperature on the reaction is investigated. Then,the most-favored condition is determined and 2-chlorobenzothiazole is synthesized in good yield. |
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| Keywords: | 2-chlorobenzothiazole 2-mercaptobenzothiazole synthesis hrichloromethyl-chlorofor-mate |
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