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水热合成法制备高纯度轻质氧化镁
引用本文:姜润田,于洁玫,黄太仲,张振伟,孙国新.水热合成法制备高纯度轻质氧化镁[J].洛阳师范学院学报,2013,32(2):66-68.
作者姓名:姜润田  于洁玫  黄太仲  张振伟  孙国新
作者单位:济南大学化学化工学院,山东济南,250022
摘    要:以卤片和尿素为原料,采用水热合成法制备了高纯度轻质氧化镁,并对工艺条件的影响因素进行分析.结果表明,当卤片与尿素的配比为1∶4.5、反应时间为5 h、反应温度为125℃、洗涤水温度为95℃的条件下制备的氧化镁,转化率高、产品质量好,可达到分析纯轻质氧化镁的标准.

关 键 词:水热合成  高纯度  轻质氧化镁

Preparation of Lightweight and High Purity Magnesium Oxide
JIANG Run-tian , YU Jie-mei , HUANG Tai-zhong , ZHANG Zhen-wei , SUN Guo-xin.Preparation of Lightweight and High Purity Magnesium Oxide[J].Journal of Luoyang Teachers College,2013,32(2):66-68.
Authors:JIANG Run-tian  YU Jie-mei  HUANG Tai-zhong  ZHANG Zhen-wei  SUN Guo-xin
Institution:(School of Chemistry and Chemical Engineering,University of Jinan,Jinan 250022,China)
Abstract:Lightweight and high purity magnesium oxide was prepared by hydrothermal method with magnesi- um chloride and urea as raw materials. The process condition and the influence factors were discussed and analyzed in our study. The result shows that most suitable reaction conditions are : the reaction ratio is 1:4.5, The reaction time is 5 h, the reaction temperature is 125℃ and the temperature is 95℃ of washing water. The products we pre- pared have the merit of high conversion and good quality. The analysis of samples shows that our pure and light- weight products reaches the magnesium oxide standard.
Keywords:hydrothermal method  high purity  lightweight magnesium oxide
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