噻吩修饰的四苯乙烯衍生物的合成 |
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引用本文: | 王静,余欢,刘澜涛.噻吩修饰的四苯乙烯衍生物的合成[J].商丘师范学院学报,2014(6):39-41. |
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作者姓名: | 王静 余欢 刘澜涛 |
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作者单位: | 商丘师范学院化学化工学院;商丘市第二高级中学; |
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基金项目: | 国家自然科学基金资助项目(21302120);河南省教育厅科学技术研究重点项目(13A150826) |
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摘 要: | 以4-溴二苯甲酮为起始原料,经McMurry反应和Suzuki偶联反应,合成出新型噻吩修饰的四苯乙烯衍生物TPE-T(a-b)和TPE-2T(a-b).新化合物的结构经1H NMR,13C NMR,MS及元素分析表征.新化合物表现出独特的聚集诱导发光现象.
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关 键 词: | 四苯乙烯 噻吩 聚集诱导发光 |
Synthesis of tetraphenylethene derivatives modified by thiophene |
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Institution: | WANG Jing , YU Huan, LIU Lantao(1. College of Chemistry and Chemical Engineering, Shangqiu Normal University, Shangqiu 476000, China; 2. Shangqiu Second Senior High School, Shangqiu 476000, China) |
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Abstract: | Tetraphenylethene derivatives TPE - T ( a - b) and TPE - 2T ( a - b ) were successfully synthesized by McMurry and Suzuki coupling reaction from 4 - bromobenzophenone. The structures of new compounds were characterized by 1 H NMR, 13C NMR, MS and elemental analysis. The new compounds exhibit the novel feature of aggregation - induced emission. |
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Keywords: | tetraphenylethene thiophene aggregation - induced emission |
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