| 2,5-己二酮的合成 |
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| 引用本文： | 严德鹏,王小勇,蒋小平,郑建新.2,5-己二酮的合成[J].湖南科技学院学报,2005,26(11):135-136. |
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| 作者姓名： | 严德鹏 王小勇 蒋小平 郑建新 |
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| 作者单位： | 湖南科技学院,生命科学与化学工程系,湖南,永州,425006 |
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| 基金项目： | 湖南科技学院课题（院字（2003）81号） |
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| 摘 要： | 本文通过乙酰乙酸乙酯的电解偶联再水解脱羧合成了2,5-己二酮,探讨了脱羧条件对2,5-己二酮产率的影响,总产率达53.5%.
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| 关 键 词： | 乙酰乙酸乙酯 2 5-己二酮 合成 电解偶联 脱羧 |
| 文章编号： | 1673-2219(2005)11-0135-02 |
| 收稿时间： | 06 27 2005 12:00AM |
| 修稿时间： | 2005年6月27日 |
Synthesis of 2,5-Hexanedione |
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| YAN De-peng,WANG Xiao-yong,JIANG Xiao-ping,ZHENG Jian-xin.Synthesis of 2,5-Hexanedione[J].Journal of Hunan University of Science and Engineering,2005,26(11):135-136. |
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| Authors: | YAN De-peng WANG Xiao-yong JIANG Xiao-ping ZHENG Jian-xin |
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| Institution: | Department of Life Science and Chemical Engineering, Hunan University of Science and Engineering, Yongzhou Hunan 425006, China |
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| Abstract: | 2,5-Hexanedione was preparated by electrolytic coupling of ethyl acetoacetate, and then hydrolysising, decarboxylating. The influence of the decarboxylatic condition to the 2,5-Hexanedione yield was investigated. The all yield is to 53.5%. |
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| Keywords: | ethyl acetoacetate 2 5-Hexanedione synthesis electrolytic oxidative coupling decarboxylation |
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