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气相色谱-质谱联用法分析奶及乳制品中的脂肪酸
引用本文:侯冬岩,回瑞华,徐丽丽,刘晓媛,李学成.气相色谱-质谱联用法分析奶及乳制品中的脂肪酸[J].鞍山师范学院学报,2007,9(4):36-38.
作者姓名:侯冬岩  回瑞华  徐丽丽  刘晓媛  李学成
作者单位:1. 鞍山师范学院,化学系,辽宁,鞍山,114007;辽宁师范大学,化学化工学院,辽宁,大连,116029
2. 辽宁师范大学,化学化工学院,辽宁,大连,116029
3. 鞍山师范学院,化学系,辽宁,鞍山,114007
基金项目:鞍山市科学技术局资助课题
摘    要:对奶及乳制品中脂肪酸的组成和含量进行测定.采用哥特里-罗兹法提取奶及乳制品中的脂肪油,氢氧化钾-甲醇溶液法甲酯化,以气相色谱-质谱联用仪进行了分析,结果表明奶及乳制品中的脂肪酸主要以碳8到碳24的脂肪酸为主,各脂肪酸在不同类型的奶及乳制品中含量也不相同.

关 键 词:奶及乳制品  脂肪酸  气相色谱-质谱联用  分离鉴定

Analysis of Fatty Acids in Milk and Dairy Products by GC/MS
HOU Dong-yan,HUI Rui-hua,XU Li-li,LIU Xiao-yuan,LI Xue-cheng.Analysis of Fatty Acids in Milk and Dairy Products by GC/MS[J].Journal of Anshan Teachers College,2007,9(4):36-38.
Authors:HOU Dong-yan  HUI Rui-hua  XU Li-li  LIU Xiao-yuan  LI Xue-cheng
Abstract:To determine the fatty acids in milk and dairy products.The fatty oils of milk and dairy products were extracted by Rose-Gettlieb method,the fatty acids in the fatty oils were esterified by potassium hydroxide-methanol,and then analyzed by gas chromatography-mass spectrometry(GC/MS).The results indicate that main fatty acids' carbon chain were from 8 to 24,each fatty acid has different conent in different samples and the content was determined by area normalization.
Keywords:Milk and dairy products  Fatty acid  GC/MS  Separation and identificaton
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