| 3,6-二甲基哒嗪的合成 |
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| 引用本文： | 辛炳炜.3,6-二甲基哒嗪的合成[J].德州学院学报,2007,23(6):37-38,44. |
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| 作者姓名： | 辛炳炜 |
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| 作者单位： | 德州学院化学系,山东德州,253023 |
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| 摘 要： | 为填补国内市场空白,以乙酰乙酸乙酯、钠为原料;通过关环、脱氢等反应,高产率地合成了3,6-二甲基哒嗪.该方法步骤短,收率高,是合成3,6-二甲基哒嗪的一种简捷方法.
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| 关 键 词： | 3 6-二甲基哒嗪 4 5-二氢-3 6-二甲基哒嗪 2 5-己二酮 合成 |
| 文章编号： | 1004-9444（2007）06-0037-02 |
| 收稿时间： | 2007-07-24 |
| 修稿时间： | 2007-07-242007-11-25 |
Synthesis of 3,6-dimethylpyridazine |
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| XIN Bing-wei.Synthesis of 3,6-dimethylpyridazine[J].Journal of Dezhou University,2007,23(6):37-38,44. |
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| Authors: | XIN Bing-wei |
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| Institution: | Department of Chemistry, Dezhou University, Dezhou Shandong 253023, China |
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| Abstract: | In order to resolve the problem which 3,6-dimethylpyridazine can't be bought from domestic market,we prepare this compound by three steps from CH3COCH2COOCH2CH3 via cyclization with hydrazine hydrate and dehydrogenation reactions.The synthetic route is a excellent method to 3,6-dimethylpyridazine.Its structure was characterized by1H NMR and MS-ESI. |
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| Keywords: | 3 6-dimethylpyridazine 4 5-dihydro-3 6-dimethypyridazine 2 5-hexadione synthesis |
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