共查询到20条相似文献，搜索用时 140 毫秒
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利用高温固相反应法,使用Fe_3O_4、Co_2O_3和Cr_2O_3为原料,制备了Cr掺杂的Co_(1-x)Cr_xFe_2O_4(x=0.10,0.15,0.20,0.25)粉末,对不同掺杂量的样品使用X射线衍射仪和扫描电子显微镜进行结构和形貌的表征,同时对样品进行了电催化析氧活性测试.结果表明,随着Cr掺杂量的增加,样品的晶格常数逐渐减小.当掺杂量为x=0.1时,样品具有最高的电催化析氧活性,在电流密度为10 mA/cm~2时,其析氧过电位为338 m V,塔费尔斜率为47 mV/dec. 相似文献
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一、金属氧化物催化剂 我们对Co_2O_3、Fe_2O_3等多种氧化物在同等条件下进行氨的催化氧化试验。实验情况如下: 相似文献
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一、实验前的准备 1.催化剂:把Fe_2O_3或Cr_2O_3(用重铬酸铵加热分解)约30克分别盛放在蒸发皿内用水调成糊状,把铜片浸入Cr_2O_3糊中把铁片浸入Fe_2O_3糊中,使金属全部沾满药粉,然后分别放入烘箱内烘干,取出放入硬质反应管内,两头塞上少量的石棉绒和单孔导气管,管外绕上电热丝,接上电源。 2.蒸馏烧瓶:一只加入浓氨水20ml,装上双连球,另一只加入浓H_2SO_4 10ml,装上单孔导气管。 相似文献
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对于不同类型的题目,要尽量避免繁杂的计算过程,简捷的解题方法是提高解题效率所必备的。 一、质量守恒法 例 在高温条件下,1.0克Fe_2O_3,和CuO的混合物被足量CO还原后得到固体混合物为0.78克。求原混合物Fe_2O_3,和CuO各多少克? 解析 该题涉及到两个化学方程式,根据化学 相似文献
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《浙江大学学报(A卷英文版)》2017,(3)
目的:通过对混合丁烯氧化脱氢过程进行反应表征,对由Zn Fe_2O_4和Co_9Bi_1Fe_3Mo_(12)O_(51)组成的双床层催化剂体系中存在的协同机理进行解释;将异构化反应过程纳入反应体系,得出混合丁烯转化率和丁二烯收率上升的原因。创新点:1.提出基于丁烯异构体在床层之间浓度重分布和异构化效应抑制作用的协同作用机理;2.设计验证实验,从直观角度证实机理,并优化了催化剂的装填量和装填顺序。方法:1.通过单一丁烯和混合丁烯的氧化脱氢反应,对单一催化剂和双床层催化剂进行反应评估,得到相关反应数据;2.通过设计对比实验,从改变参加反应物质的直观角度对协同机理进行验证和解释;3.对参加反应的双层床催化剂中两种催化剂的装填量和装填顺序进行优化,为进一步研究组合型催化剂提供实验基础。结论:1.Zn Fe_2O_4对两种2-丁烯有更优的催化效果,而Co_9Bi_1Fe_3Mo_(12)O_(51)对1-丁烯有更优的催化效果,由两者组成的双层床催化体系对单一丁烯和混合丁烯的反应效果都有所提升,证明两种催化剂之间存在协同效应。2.双层床催化剂体系中,两种催化剂之间的协同作用机理是:催化剂不同活性导致丁烯异构体在床层之间的浓度发生重分布,同时由于多种异构体同时存在抑制了异构化反应。3.对双层床催化剂体系的装填顺序和装填量的优化结果表明,Zn Fe_2O_4装填在上层,Co_9Bi_1Fe_3Mo_(12)O_(51)装填在下层,且两者比例处于4:6到6:4之间时催化效果最佳。 相似文献
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《中学生数理化(高中版)》2010,(4)
某工厂废水中含有5.00×10~(-3) mol·L~(-1)Cr_2O_7~(2-),其毒性较大.某研究性学习小组为了变废为宝,将废水处理得到磁性材料Cr_(0.5)Fe_(1.5)FeO_4(Fe的化合价依次为+3、+2价),设计了如下实验: 相似文献
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现行初三化学课本P120有CO还原CuO的实验,高中课本有CO还原Fe_2O_3的实验,实验过程中都存在着下列缺点:①课前准备和课 相似文献
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第一种,定复杂分子系数为1的方法。例1.Al+Fe_3O_4——Al_2O_3+Fe步骤:1.住主要矛盾,确定复杂分子式 Fe_3O_4(Al_2O_3亦可)前面系数为1。2.根据反应前后各元素(或原子团)的原子个数相等的原则进行配平。配平的顺序写在分子式下面 相似文献
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谭寿文 《华南师范大学学报(社会科学版)》1978,(12)
下面介绍两种通过实践证明学生容易接受,方法简便而且适用范围较广的化学方程式的配平方法.第一种,定复杂分子系数为1的方法.例1.Al+Fe_3O_4——Al_2O_3+Fe步骤:1.抓主要矛盾,确定复杂分子式Fe_3O_4(Al_2O_3亦可)前面系数为1;2.根据反应前后各元素(或原子团)的原子个数相等的原则进行配平.配平的顺序写在分子式下面:3.分子式前面不分数,各为能分子式的系数分别×3,使系数都成整数. 相似文献
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《海外英语》2007,(4):36
There are numbers of crossroads on our long and unpredictable life journey where we totally have no idea about which direction to choose. No matter what our decision is, we should not turn back, but face the music and go ahead instead. I am this kind of girl who always does try without regretting, one example is how I dealt with my love. 相似文献
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Migration occurs behind a variety of reasons and has a great effect on the whole world. People may migrate in order to improve their economic situation, or in order to escape civil strife, persecution, and environmental disasters. The impact of migration is complex, bringing both benefits anddisadvantages. This paper briefly talks about the causes of migration, the allocation of benefits, and the ways in which individual countries and the international community deal with this important subject. 相似文献
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Sister Carrie is one of the most controversial characters in American literature.Thought as a "fallen woman" firstly,she was defined as a "new woman" by some critics later. However, by digging into the motivaton behind the whole process of Carrie's "success", the relationship between Carrie and her creator (the author), the social conditions of then American, it can be found that Carrie has never been free-standing on her thought and she has never found her real-sdf even after becoming a famous actress. In a society dominated by mass consumerism Carrie is only an adherent of her own desires. She also is a representative of all those country girls flooded into cities, a symbol and a sacrifice of the urbanization of America in a time countryside was overcome by cities. 相似文献
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RUZBEHANI Mohsen 《重庆大学学报(英文版)》2004,3(1):20-25
1.IntroductionOne-cyclecontrolmethod,whichwasproposedaboutonedecadeago[1],hasbecomeanattractivemethodinspecialfieldssuchaspowerfactorcorrection[2-6],switchingamplifiers[7,8],etc.Themainideaofthiscontrollerisbasedonintegrationofdiodevoltageinone-cycleandforcesittobeexactlyequaltothereferencevalue.Themainadvantageofthiscontrollerisitsrealtimeabilitytorejectthevariationofinputvoltage[1].Despitethisgreatability,ithasnogoodperformancesinrejectingofloaddisturbanceandfollowingreferencecommands.Espec… 相似文献
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Rajesh Kanoi 《海外英语》2007,(1):52
Today, Sunday morning, I sit thinking and typing at my computer. My thoughts are in my homeland, India and my body is in China. The body is here and mind there for a good reason. Mr. Hu is president and I am resident and both are in each other's countries (what a difference the absence of one small letter makes!). Mr. Hu will return in a few days and I will stay on longer. 相似文献
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正A One day a pig went to the stable(马棚)to see his good friend,an oldhorse,and was going to stay there forthenight.Night came and it was time forsleep.The pig went into the straw heap(稻草堆)and lay comfortably.A longtime passed,but the horse was stillstanding there and did not move.Thepig asked the horse why he did not go tosleep."Standing like this is the begin-ning ofsleeping,"answered the horse. 相似文献
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《今日中学生》2014,(9)
正1.Any fool can count the seeds in an apple.Only God can count all the apples in one seed.2.Happy families are all alike;every unhappy family is unhappy in its own way.3.Memories are the key not to the past,but to the future.4.Sometimes in the dark you see what you want to see.5.There is a great difference between 相似文献
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《重庆大学学报(英文版)》2014,(2)
正Scope and Policy The Journal of Chongqing University-English Edition(JCQU-E)is a peerreviewed journal publishing research articles in multiple disciplines of science and technology,covering civil and environmental engineering,chemical engineering,biotechnology,mechanical and electrical engineering,computer and data processing,mining,metallurgy,materials science,and interdisciplines thereof. 相似文献