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《昆明师范高等专科学校学报》2014,(3)
采用自动电位滴定法测定焊剂中氯离子的质量分数,对试样的处理、酸度的影响、线性范围、标准回收、精密度和准确度等进行探究.结果表明:对样品11次测定值的相对标准偏差(RSD)为2.27%~2.35%,标准回收率为99.00%~100.80%;所用方法的准确度和精密度较好,适合于焊剂中0.02%~1.00%氯离子的测定. 相似文献
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通过复混肥的检测实践,对标准GB/T8572,8573,8574中确定各养分称取试样范围,N试样处理,N蒸馏方法分别进行一定探讨.利用数理统计方法以复混肥(含量≥25%)为原材料,进行不同称量处理,结果表明测定N,P,K称取复混肥量分别以1 g,1 g,2 g所得测定值能代表该肥料的准确含量;同时对N试样采取何种处理提出见解. 相似文献
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采用硫酸溶解试样,以铜离子为催化剂,以硫脲为还原剂,基于钼(V)与硫氰酸盐生成橙红色络合物,建立了钛及钛合金中钼量的硫氰酸盐分光光度法.对试验条件如催化剂、还原剂、显色剂溶液用量进行了优化,同时考察了最大吸收波长、溶解酸种类、共存离子、显色体系酸度对钼测定的影响.在最佳试验条件下,钼含量在0.10%~16.0%范围内与其吸光度值成线性关系.按照试验方法开展了加标回收试验,回收率为96.4%~103.1%;并对6种钛合金试样进行钼含量测定,相对标准偏差(RSD,n=11)为0.7%~2.0%,测试结果与ICP-AES法测定一致. 相似文献
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为优选钙片中钙含量测定方法,对EDTA法、高锰酸钾法和分光光度法测定钙片中钙,从测定过程、与标示值比较和置信区间的比较三个方面进行了实验研究,结果表明3种方法均可用于钙片中钙含量的测定。综合测量结果准确度和方法的精密度因素,得出定量分析中试样的处理过程对测定结果产生的影响不容忽视。 EDTA法较其他两种方法具有操作简便、快速等优点,尤其是用直接称量取样的方法获得测量试样避免了稀释过程量器体积产生的误差,测定值较分光光度法和高锰酸钾法更接近标示值,可作为补钙药物中钙含量测定的首选方法。 相似文献
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将试样干粉末采用混酸(HNO3:HClO4=4:1)消解,用火焰原子吸收法连续测定其中的铜、锌、铁、钙、铅.该方法测定相对标准偏差小于0.3779%,样品回收率为95%~105%.结果满意. 相似文献
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葛根样品的不同消解方法进行了探讨,提出了用微波消解电感耦合等离子体发射光谱法(ICP-AES)测定葛根中微量元素锌的方法。测定方法的检测下限达0.005μ/ml.方法的相对标准偏差穴RSD雪为2.7%。试样经过微波消解后,测定的平均回收率为101.2%,具有灵敏、准确及快速测定的特点。 相似文献
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李萍 《中国科教创新导刊》2014,(10):182-182
本文在测定双氧水的质量分数时,分别采用了量取法和称量法移取试样,并对所测得的数值进行分析比较,得知,称取法移取试样测得的双氧水质量分数准确度好于量取法移取试样测得的值。 相似文献
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《海外英语》2007,(5):10-11
Many college freshmen arrive woefully unprepared to do college work, and as disadvantaged populations continue to grow, the share of the American work force that has made it through college is expected to plummet. Many experts blame that educational failure not just on high schools but also on colleges. School & College, a special report by The Chronicle, looks at efforts to fix the system. What reforms would better prepare students for college? What should schools and colleges be doing differently? How should state and federal officials help? 相似文献
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《海外英语》2007,(4):36
There are numbers of crossroads on our long and unpredictable life journey where we totally have no idea about which direction to choose. No matter what our decision is, we should not turn back, but face the music and go ahead instead. I am this kind of girl who always does try without regretting, one example is how I dealt with my love. 相似文献
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邱崇丙 《唐山师范学院学报》2014,(1):21-23
汉字的六书,《说文》对“转注”一类,语焉不详。后世学者提及转注,也仅限于许慎所举出的例字。《汉字例说》一文,作者从转注的角度综合考虑,对部分现代常用字作了分析,跟传统的解释有所不同。希望能抛砖引玉,互相切磋,以推进学术研究。 相似文献
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Migration occurs behind a variety of reasons and has a great effect on the whole world. People may migrate in order to improve their economic situation, or in order to escape civil strife, persecution, and environmental disasters. The impact of migration is complex, bringing both benefits anddisadvantages. This paper briefly talks about the causes of migration, the allocation of benefits, and the ways in which individual countries and the international community deal with this important subject. 相似文献
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Sister Carrie is one of the most controversial characters in American literature.Thought as a "fallen woman" firstly,she was defined as a "new woman" by some critics later. However, by digging into the motivaton behind the whole process of Carrie's "success", the relationship between Carrie and her creator (the author), the social conditions of then American, it can be found that Carrie has never been free-standing on her thought and she has never found her real-sdf even after becoming a famous actress. In a society dominated by mass consumerism Carrie is only an adherent of her own desires. She also is a representative of all those country girls flooded into cities, a symbol and a sacrifice of the urbanization of America in a time countryside was overcome by cities. 相似文献
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RUZBEHANI Mohsen 《重庆大学学报(英文版)》2004,3(1):20-25
1.IntroductionOne-cyclecontrolmethod,whichwasproposedaboutonedecadeago[1],hasbecomeanattractivemethodinspecialfieldssuchaspowerfactorcorrection[2-6],switchingamplifiers[7,8],etc.Themainideaofthiscontrollerisbasedonintegrationofdiodevoltageinone-cycleandforcesittobeexactlyequaltothereferencevalue.Themainadvantageofthiscontrollerisitsrealtimeabilitytorejectthevariationofinputvoltage[1].Despitethisgreatability,ithasnogoodperformancesinrejectingofloaddisturbanceandfollowingreferencecommands.Espec… 相似文献
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Rachel Zupek 《海外英语》2007,(11):40-41
我们绝大部分人都同意一件事情——我们喜欢金钱。但是你对金钱的喜欢之情足够到让你创立一份事业么?.财富通常被人忽视,主要在于人们不能真正了 相似文献