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1.
氟电极毫伏值数据转换方法研究   总被引:1,自引:0,他引:1  
改进、统一、量化氟电极毫伏值转换为样品氟含量数据处理方法,使各种样品的氟化物测定结果更接近真值,方法间的测定结果具有可比性;选用标准加入法、标准加入微量曲线法、标准加入常量曲线法,对氟离子选择电极测得毫伏值转换为样品氟含量的数据处理方法进行了研究和改进;改进后方法的回收率达99%;变异系数小于2.73%氟离子选择电极测定微量氟不仅实验方法要定标准,而其测定所得毫伏值转换为样品氟含量的数据处理方法也应规定统一的标准。  相似文献   

2.
农民的养鱼塘 ,偶尔会出现鱼大面积的死亡。在现实生活中还会发生因食用含有农药的蔬菜而中毒的事故。怎样判断水或蔬菜中含有农药 ?在多次实验后 ,我们总结出如下较简便的检测农药的方法。1 有机磷农药的快速测定1.1 测定原理水中的有机磷农药经溴氧化后与刚果红作用 ,会生成深蓝色物质 ,这可以鉴定样品中是否存在有机磷农药。1.2 检测方法(1)水样的检测将水样注入试管中占试管体积约 2 / 5 ,加入饱和溴水一毫升 ,撕半条刚果红试纸放入试管中 ,将试管加热 ,刚果红试纸变蓝色 ,说明水样中含有机磷农药。刚果红试纸为橙黄色 ,说明水样中不…  相似文献   

3.
土壤中有效磷快速测定方法的研究   总被引:1,自引:0,他引:1  
采用试纸法测定土壤中有效磷的含量,通过加入钼酸铵、酒石酸钠、抗坏血酸和硫酸的量对显色结果影响进行了研究,并利用组装的便携式磷酸根测定仪对土壤中有效磷测定方面的应用进行了探索。结果表明:试纸法检测范围为0.1~1.2μg/m L,基本能满足常规土壤中有效磷的快速测定;组装的便携式磷酸根测定仪测得的磷标准曲线线性关系较好,其相关性R2为0.9995,因此可准确的测定土壤中磷酸根浓度,进而快速求得土壤中有效磷含量。  相似文献   

4.
对用国标法——盐酸萘乙二胺分光光度法测定食品中的亚硝酸盐含量的影响因素进行了研究。通过单因素实验,分析了三种因素—显色时间、显色温度、样品pH值等对测定结果的影响。结果表明,显色温度、显色时间和样品pH值等因素均对检测结果都有一定的影响,提出了在实际应用中对检测方法的改进措施。  相似文献   

5.
标准曲线绘制是临床生物化学检验工作中进行物质定量检测的基本要求。绘制标准曲线的方法很多,本文介绍了采用平均K值法绘制标准曲线的方法,并同其它方法比较。提示本方法具有灵敏准确、快速简便的特点。  相似文献   

6.
对过硫酸钾消解法绘制污水中总磷标准曲线方法进行改进,水样取样量和所加入试剂的用量均同步缩小至1/10,并于北京双晖京承公司的CM-05型多功能水质监测仪的COD消解管中进行显色反应,另在与之配套的分光光度计上直接比色测定,消解时间仅为15 min,具有快捷、简便、高效等优点.  相似文献   

7.
应用茚三酮显色法对蛋白质水解度的测定及其标准曲线生成进行了分析。进而,基于一元线性回归分别在Excell和Matlab平台上对标准曲线的生成进行了研究,并给出了相应的标准曲线生成源代码,为蛋白质水解度的控制及工业分析中各标准曲线的绘制提供了必要的手段和方法。  相似文献   

8.
分别用火焰原子吸收法和1,10-菲啰啉分光光度法测定铬铁废液中铁的总量.绘制了两种方法的标准曲线,测定了空白值、加标回收率和标准样品.两种方法的空白值都比较稳定,相关性以及斜率等数值都很接近,它们的准确度都比较好,相对标准偏差分别为1.2%和2.6%.两者的平均回收率分别为108%和94%,基本符合实验要求.因此,两种方法的测定结果都在真值允许范围内,它们的标准曲线,精密度和准确性都比较好.两种方法的结果通过t检验,无显著性差异.两者都适用于低浓度的铁溶液,但分光光度法灵敏度稍高.  相似文献   

9.
粘度法是测定高分子化合物相对分子质量的一种简单易行的方法,由于在此实验中会遇到许多对实验结果产生影响的因素。对在30℃时测定聚乙二醇水溶液粘度的实验进行了改进,利用逐步加入乙二醇水溶液,而不需要清洗干燥Ubbelohde式粘度计。结果表明节约了时间,同时得到较好的实验结果。  相似文献   

10.
比色皿质量直接关系到比色分析的准确度,但对比色皿的质量监测国内尚乏报道,兹将我们的监测结果报告如下: 材料与方法 器材微米千分尺(哈尔滨量具厂),721分光光度计及比色皿(上海第三分析仪器厂)。  相似文献   

11.
汉字倒说     
汉字的六书,《说文》对“转注”一类,语焉不详。后世学者提及转注,也仅限于许慎所举出的例字。《汉字例说》一文,作者从转注的角度综合考虑,对部分现代常用字作了分析,跟传统的解释有所不同。希望能抛砖引玉,互相切磋,以推进学术研究。  相似文献   

12.
《海外英语》2007,(5):44-45
It is worthy of noting that, whilst Crookston Castle witnessed the earlier and happier portion of Mary's variegated life,  相似文献   

13.
钱生钱!     
我们绝大部分人都同意一件事情——我们喜欢金钱。但是你对金钱的喜欢之情足够到让你创立一份事业么?.财富通常被人忽视,主要在于人们不能真正了  相似文献   

14.
《海外英语》2007,(4):36
There are numbers of crossroads on our long and unpredictable life journey where we totally have no idea about which direction to choose. No matter what our decision is, we should not turn back, but face the music and go ahead instead. I am this kind of girl who always does try without regretting, one example is how I dealt with my love.  相似文献   

15.
The problem on the geometrc inequalities involving an n-dimensional simplex and its inscribed simplex is studied. Aninequality is established, which reveals that the difference between the squared circumradius of the n-dimensional simplex andthe squared distance between its circumcenter and barycenter times the squared circumradius of its inscribed simplex is not lessthan the 2(n-1)th power of n times its squared inradius, and is equal to when the simplex is regular and its inscribed siplex is atangent point one. Deduction from this inequality reaches a generalization of n-dimensional Euler inequality indicating that thecircumradius of the simplex is not less than the n-fold inradius. Another inequality is derived to present the relationship betweenthe circumradius of the n-dimensional simplex and the circumradius and inradius of its pedal simplex.  相似文献   

16.
王菲 《华章》2007,(12):273-273
Migration occurs behind a variety of reasons and has a great effect on the whole world. People may migrate in order to improve their economic situation, or in order to escape civil strife, persecution, and environmental disasters. The impact of migration is complex, bringing both benefits anddisadvantages. This paper briefly talks about the causes of migration, the allocation of benefits, and the ways in which individual countries and the international community deal with this important subject.  相似文献   

17.
现在,我们可以没有面包,没有钱,没有房子,没有车子……但我们唯独不能丢失的是高尚的情操,笃定的信念,还有,满满的希望!  相似文献   

18.
Using virtual reality for interactive design gives a designer an intuitive vision of a design and allows the designer to achieve a viable, optimal solution in a timely manner. The article discusses the process of making the Virtual Reality System of the Humble Administrator's Garden. Translating building data to the Virtual Reality Modeling Language (VRML) is by far unsatisfactory. This creates a challenge for computer designers to do optimization to meet requirements. Five different approaches to optimize models have been presented in this paper. The other methods are to optimize VRML and to reduce the file size. This is done by keeping polygon counts to a minimum and by applying such techniques as object culling and level-ofdetail switching.  相似文献   

19.
钱微 《华章》2007,(3):124-124
The awareness of individualism can be traced back to the period of American Revolution when the Declaration of Independence was produced.It expressed basic beliefs concerning freedom,equality,democracy,privacy and the relationship between people and government,which were exactly what the philosophy of individualism mostly dealt with at that time.This paper is to exploit the essence of individualism by analyzing the Declaration .The analysis enables us to reconsider its significance to the issue of America human rights and foreign policies.  相似文献   

20.
裴水妹 《华章》2007,(11):196
Sister Carrie is one of the most controversial characters in American literature.Thought as a "fallen woman" firstly,she was defined as a "new woman" by some critics later. However, by digging into the motivaton behind the whole process of Carrie's "success", the relationship between Carrie and her creator (the author), the social conditions of then American, it can be found that Carrie has never been free-standing on her thought and she has never found her real-sdf even after becoming a famous actress. In a society dominated by mass consumerism Carrie is only an adherent of her own desires. She also is a representative of all those country girls flooded into cities, a symbol and a sacrifice of the urbanization of America in a time countryside was overcome by cities.  相似文献   

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