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1.
郜洪文 《科技通报》1995,11(4):221-224
本文研究β修正光度法测定工业废水中痕量砷,它能消除过量BRB的干扰提高分析敏度、精密度和准确度。结果表明砷浓度0-0.40mg/L时,修正吸光度有良好线性关系,检出限0.004mg/L,加标回收率93.0%-111%,相对标准偏差RSD≤6.5%,该方法适合于化工废水、城市污水及各种环境水质分析。  相似文献   

2.
本文系统地研究了甲硝唑在汞电极上的电极过程,证明了该电极过程为一含有吸附作用的不可逆的扩散控制过程,电子转移数为4,不可逆系数a=0.714.建立了甲硝唑的单扫示波极谱测定法,在0.20mol/L的NaCl溶液中,于-0.71V(vsSCE)处的峰高与浓度[(0.02─80)mg/L]间存在良好的线性关系,检测限为2.4μg/L,RSD=2.0%(n=8),并考察了人体内常见微量物质对的影响。  相似文献   

3.
黄芩甙的极谱研究   总被引:1,自引:0,他引:1  
用单扫示波极谱法研究了黄芩甙的电化学特性.在0.05mol/L柠檬酸钠+0.2mol/LHCl底液中,黄芩甙于-1.16V(P1)和-1.34V(P2)(vs.SCE)处产生两个二阶导数峰,前者为黄芩甙分子的还原波,后者为其一价阴离子的还原波,均为羰基的双电子还原波.利用峰P1可测定黄芩甙,线性范围为0.16~0.64mg/L和0.72~24mg/L,检测限为0.08mg/L.将该法用于中药黄芩中黄芩甙的测定时,获得满意结果  相似文献   

4.
茶多酚抗突变和消除自由基作用的研究   总被引:6,自引:0,他引:6  
曹明富  袁妙葆 《科技通报》1994,10(5):301-305
采用E.ColiSOS显色法,小鼠骨髓细胞微核及染色体畸变试验和体外自由基消除实验等方法测定了茶多酚复合物(TP)的抗突变和消除自由基作用.结果表明:(1)TP的终浓度在2.5和5mg/ml时,对由阳性致突变物MNNG,EMS和NaN_3诱导的SOS应答反应均具有明显的抑制作用;(2)小鼠每日ig40、80和120mg/kg剂量的TP能明显抑制由环磷酰胺(CP)诱发的骨髓PCE的MNCF,三种剂量TP的抑制率分别为40.98%、66.76%和65.94%;(3)TP对MMC诱发的骨髓细胞染色体畸变(CA)的抑制率分别为62.56%、55.71%和47.95%;(4)在X/XO-ESR、X/XO/Luminol-BCL和IR/NBT-SPM三种模型中TP对超氧阴离子O_2自由基均具有极强的消除作用,消除率分别为98±6%、98±1.2%和95±1.5%,对O_2的消除效率明显强于维生素C和E,对不同工艺制备的TP消除活性氧自由基作用的测定结果显示:脱咖啡碱程度高,EGC和L-EGCG含量比例高的TP-3制剂消除O_2的效率最高.因此,TP消除有害自由基,中断或终止自由基的氧化反应是抗突变,抗肿瘤作用的主要机制  相似文献   

5.
一阶导数光谱法测定杞菊地黄丸中丹皮酚含量   总被引:2,自引:0,他引:2  
杞菊地黄丸为滋肾养肝药,由八种中药组成,本文采用一阶导数光谱法,不经分离对丹皮酚进行含量测定,实验证明,用△A=A267-A263测定其含量较准确,在3.018~8.048mg/ml浓度范围内呈良好线性关系,回归方程A=0.003724+0.01406C、r=0.9996,回收率为101.95%(RSD=1.74%n=5)。  相似文献   

6.
朱岩  李刚 《科技通报》1994,10(5):297-300
采用梯度淋洗离子色谱法对碱金属、碱土金属及其铵类进行分析,该方法采用CG3分离柱,0.3mmol/LHCl为淋洗剂,4min后改用3.0mmol/L盐酸间苯二胺和5.0mmo1/LHCl作淋洗剂(流速2.0ml/min)采用微膜抑制柱,再生液为50mmol/LKOH(流速2.0ml/min),用电导检测法分别检测Li ̄+、Na ̄+、NH、K ̄+和Mg ̄(2+)、Ca ̄(2+)、Sr ̄(2+)、Ba ̄(2+).对分析条件进行了探讨.  相似文献   

7.
本试验采用西藏著名野生花卉蓝玉簪龙胆茎段为组织培养材料,通过多次试验后确定:蓝玉簪龙胆的启动培养中适宜的培养基为;MS+NAA0.5(mg/1,激素单位下同)+BA0.5-1.0,每茎段平均分化形成4.2个芽;诱导愈伤组织的适宜培养基为MS+BA0.5+NAA0.5-1.0;  相似文献   

8.
乳清酸的单扫示波极谱研究   总被引:1,自引:0,他引:1  
乳清酸在0.1mol/LHClO4+0.02mol/LNaClO4底液中,于JP-2型示波极谱仪上,有一良好的二阶导数峰Ep=-0.860±0.01V(SCE),浓度在1×10-7~6×10-5mol/L范围内,与峰高成线性关系,检测限为7.5×10-8mol/L.实验证明,电极过程为具有催化性质的双电子可逆过程.  相似文献   

9.
程吟梅  张曙云 《科技通报》1995,11(6):381-383
报告108例病毒性肝炎患者血清总补体(CH_(50))和C_3值的检测结果:急性肝炎的CH_(50)为68.4±6.13单位/ml,C_3为130.2±6.67mg%,均高于正常组(CH_(50)为48.5±5.75单位/ml,C_3为102±5mg%),P<0.01;其他类型的肝炎患者组的补体均低于正常组,P<0.01.补体的含量与T细胞花环(Et花环)呈中度相关,与GPT呈高度相关,因此测定CH_(50)和C_3可作为衡量患者机体免疫功能和判断病毒性肝炎预后的指标之一。  相似文献   

10.
用超细玻璃纤维滤膜收集城市交通干道空气中的铅,硝化后使用石墨炉原子吸收分光光度法测定。本法具有灵敏度高,精密度和准确度较好等优点。铅平均浓度在10.57~66.67μg/L时,其相对偏差在0.47%~5.7%之间,标准差在0.18~0.33之间,CV在0.47%~3.03%之间,标准曲线的相关系数为0.998。  相似文献   

11.
This study examined how students who had no prior experience with videoconferencing would react to the use of videoconferencing as an instructional medium. Students enrolled in seven different courses completed a questionnaire at the beginning of the semester and again at the end of the semester. Students at the origination and remote sites did not differ in their reactions toward videoconferencing but there was a significant difference for gender. Women reacted less favorably to videoconferencing. Compared to the beginning of the semester, students reported significantly less positive attitudes toward taking a course through videoconferencing at the end of the semester. There were no significant differences in students' attitudes toward videoconferencing across courses at the beginning of the semester but there were significant differences across the courses at the end of the semester. The results suggest the need for better preparation for both students and instructors.  相似文献   

12.
Ajoint study by Prof. ZHANG Zhibin from the CAS Institute of Zoology and his co-workers from Norway, US and Swiss have indicated that historical outbreaks of migratory locusts in China were associated with cold spells, suggesting that China's projected climate warming could decrease the pest's numbers. The study was published in Proceedings of theNational Academy of Sciences on 17 September, 2007.  相似文献   

13.
A computer-mediated group is a complex entity whose members exchange many types of information via multiple means of communication in pursuit of goals specific to their environment. Over time, they coordinate technical features of media with locally enacted use to achieve a viable working arrangement. To explore this complex interaction, a case study is presented of the social networks of interactions and media use among members of a class of computer-supported distance learners. Results show how group structures associated with project teams dominated who communicated with whom, about what, and via which media over the term, and how media came to occupy their own communication niches: Webboard for diffuse class-wide communication; Internet Relay Chat more to named others but still for general communication across the class; and e-mail primarily for intrateam communication. Face-to-face interaction, occurring only during a short on-campus session, appears to have had a catalytic effect on social and emotional exchanges. Results suggest the need to structure exchanges to balance class-wide sharing of ideas with subgroup interactions that facilitate project completion, and to provide media that support these two modes of interaction.  相似文献   

14.
Aresearch group led by Prof. ZHAI Qiwei from the Institute for Nutritional Sciences under the CAS Shanghai Institutes for Biological Sciences has discovered that even relatively low doses of resveratrol--a chemical found in the skins of red grapes and in red wine--can improve the sensitivity of mice to the hormone insulin, according to a report in the October,2007 issue of Cell Metabolism. As insulin resistance is often characterized as the most critical factor contributing to the development of Type 2 diabetes, the findings“provide a potential new therapeutic approach for preventing or treating” both conditions, the researchers said.  相似文献   

15.
Electronic data interchange (EDI) provides means for interorganizational communication, creates network externalities, requires an advanced information technology (IT) infrastructure, and relies on standards. In the diffusion of such innovations, institutional involvement is imperative. Such institutions contain governmental agencies, national and global standardization organizations, local government, and nonprofit private organizations like industry associations. The last type of organizations we call intermediating institutions. They intermediate or coordinate ("inscribe") the activities of a group of would-be adopters. Unfortunately, little is known of how these organizations shape the EDI diffusion trajectory. In this article we examine one specific type of intermediating organizations?industry associations?and how they advanced the EDI diffusion process in the grocery sectors of Hong Kong, Denmark and Finland. We identify six institutional measures, placed into a matrix formed by the mode of involvement (influence vs. regulation) and the type of diffusion force (supply push vs. demand pull), that can be mobilized to further the EDI diffusion. Industry associations were found to be active users of all these measures to varying degrees. Their role was critical especially in knowledge building, knowledge deployment, and standard setting. Furthermore, institutional involvement varied due to policy and cultural contingencies and power dependencies.  相似文献   

16.
The increasing prospects of digital piracy has prompted the perceived need by electronic publishers to adopt technical systems of protection, and governments to reform their copyright laws. This article is a preliminary study of the management of intellectual property by electronic publishers, defined as those involved in the production of online databases, and CD-ROMs. It focuses on three main issues: (1) how electronic publishers view the increasing threat of piracy; (2) the methods of protection employed to protect intellectual property in digital format; and (3) the importance of technological protection of intellectual property in electronic publications. The analysis is based on a sample of 23 UK electronic publishers. The interviews revealed an interesting assortment of protection methods and did not show that technological protection was a preferred way. Instead, the means of protection, in addition to copyright law, comprised niche markets, pricing, trust, bad publicity, and nontechnical and technical means.  相似文献   

17.
Long-standing conflict between domain name registrants and trademark holders prompted the Internet Corporation for Assigned Names and Numbers (ICANN) to create a global, mandatory arbitration procedure known as the Uniform Dispute Resolution Policy (UDRP). The UDRP has been used in 2166 cases involving 3938 domain names as of 1 November 2000. The policy gives the initiator of a complaint, generally a trademark holder, the right to choose which ICANN-accredited dispute resolution service provider (RSP) will handle the case. During the preparation of the UDRP,some feared that complainant selection would lead to "forum shopping" that might bias the results. This article performs a statistical assessment of the forum-shopping thesis and finds support for it. There are statistically significant differences in the various RSPs' propensity to take away names from defendants; there are also major differences in the number of cases brought to each RSP. RSPs who take away names have the larger share of cases. The study examines other variables that might explain differences in market share, such as price, the plaintiff's nationality, or the time taken to decide a case. It finds that nationality and time also are correlated with market share. The study concludes that shopping for a favorable outcome is an important factor in the UDRP.  相似文献   

18.
Prof. Raymond C.K. Chen, a neuropsychologist with the CAS Institute of Psychology, has made novel progress in his studies of schizophrenia. His work has been reported by a recent issue of Behavioural Neurology.  相似文献   

19.
Active biological molecules and functional structures can be fabricated into a bio-mimetic system by using molecular assembly method. Such materials can be used for the drug delivery, disease diagnosis and therapy, and new nanodevice construction.  相似文献   

20.
<正>In Xishuangbanna,one of China’s most biodiverse regions,landscape has changed dramatically during the past three decades due to the conversion of tropical rainforest to rubber plantations.In steep areas,terraces are often constructed before planting rubber trees,which causes two important changes in the soil:the destabilization of soil in the bench terraces and the increased vulnerability of unvegetated riser faces to erosion.Few studies have documented the nature and intensity of erosion on bench terraces.Prof.LIU Wenjie and his colleagues from the Xishuangbanna Tropical Botanical Garden(XTBG)conducted a study in Menglun County(21°5′39″N,101°15′55″E),Xishuangbanna to evaluate the influence  相似文献   

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